Carbamic acid, [[9,10-dihydro-5-hydroxy-6-[(4-methoxyphenyl)methoxy]-9,10-dioxo-1,4- anthracenediyl]bis(imino-2,1-ethanediyl)]bis[[2-(triphenylmethoxy)ethyl]-, bis(1,1-dimethylethyl) ester

Base Information

Chemical Name:Carbamic acid, [[9,10-dihydro-5-hydroxy-6-[(4-methoxyphenyl)methoxy]-9,10-dioxo-1,4- anthracenediyl]bis(imino-2,1-ethanediyl)]bis[[2-(triphenylmethoxy)ethyl]-, bis(1,1-dimethylethyl) ester
CAS No.:87406-44-8
Molecular Formula:C78H80N4O11
Molecular Weight:1249.51
Hs Code.:

Carbamic acid,
[[9,10-dihydro-5-hydroxy-6-[(4-methoxyphenyl)methoxy]-9,10-dioxo-1,4-
anthracenediyl]bis(imino-2,1-ethanediyl)]bis[[2-(triphenylmethoxy)ethyl]-,
bis(1,1-dimethylethyl) ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [[9,10-dihydro-5-hydroxy-6-[(4-methoxyphenyl)methoxy]-9,10-dioxo-1,4- anthracenediyl]bis(imino-2,1-ethanediyl)]bis[[2-(triphenylmethoxy)ethyl]-, bis(1,1-dimethylethyl) ester

Chemical Property:

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Technology Process of Carbamic acid, [[9,10-dihydro-5-hydroxy-6-[(4-methoxyphenyl)methoxy]-9,10-dioxo-1,4- anthracenediyl]bis(imino-2,1-ethanediyl)]bis[[2-(triphenylmethoxy)ethyl]-, bis(1,1-dimethylethyl) ester

There total 5 articles about Carbamic acid, [[9,10-dihydro-5-hydroxy-6-[(4-methoxyphenyl)methoxy]-9,10-dioxo-1,4- anthracenediyl]bis(imino-2,1-ethanediyl)]bis[[2-(triphenylmethoxy)ethyl]-, bis(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 824-94-2
p-methoxybenzyl chloride

: 87406-42-6
5,8-bis<2-ethylamino>-1,2-dihydroxy-9,10-anthracenedione

: 87406-44-8
5,8-bis<2-ethylamino>-1-hydroxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

Guidance literature:: With potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; for 4h;
DOI:10.1246/bcsj.56.1812

Reference yield:

: 76-83-5
trityl chloride

: 87406-44-8
5,8-bis<2-ethylamino>-1-hydroxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / pyridine / 17 h / 60 °C

2: 87 percent / K₂CO₃ / dimethylformamide; CH₂Cl₂ / 4 h

With pyridine; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.56.1812

Reference yield:

: 87406-40-4
2-(t-butoxycarbonyloxy)-5,8-bis<2-(N-t-butoxycarbonyl-2-hydroxyethylamino)ethylamino>-1-hydroxy-9,10-anthracenedione

: 87406-44-8
5,8-bis<2-ethylamino>-1-hydroxy-2-(p-methoxybenzyloxy)-9,10-anthracenedione

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / pyridine / 17 h / 60 °C

2: 94 percent / K₂CO₃ / acetone / 7 h / Heating

3: 87 percent / K₂CO₃ / dimethylformamide; CH₂Cl₂ / 4 h

With pyridine; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1246/bcsj.56.1812