Benzoic acid, 2,4-bis(acetyloxy)-, 2-(phenylseleno)ethyl ester

Base Information

Chemical Name:Benzoic acid, 2,4-bis(acetyloxy)-, 2-(phenylseleno)ethyl ester
CAS No.:875544-25-5
Molecular Formula:C19H18O6Se
Molecular Weight:421.308
Hs Code.:
DSSTox Substance ID:DTXSID70471122
Nikkaji Number:J2.239.840G
Wikidata:Q82299547

Synonyms:875544-25-5;Benzoic acid, 2,4-bis(acetyloxy)-, 2-(phenylseleno)ethyl ester;DTXSID70471122

Suppliers and Price of Benzoic acid, 2,4-bis(acetyloxy)-, 2-(phenylseleno)ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzoic acid, 2,4-bis(acetyloxy)-, 2-(phenylseleno)ethyl ester

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:10
Exact Mass:422.02686
Heavy Atom Count:26
Complexity:488

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)OC1=CC(=C(C=C1)C(=O)OCC[Se]C2=CC=CC=C2)OC(=O)C

Technology Process of Benzoic acid, 2,4-bis(acetyloxy)-, 2-(phenylseleno)ethyl ester

There total 4 articles about Benzoic acid, 2,4-bis(acetyloxy)-, 2-(phenylseleno)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65275-32-3
2-(phenylselenyl)ethanol

: 50740-12-0
2,4-diacetoxybenzoyl chloride

: 875544-25-5
2,4-diacetoxy-benzoic acid 2-phenylselanyl-ethyl ester

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1248/cpb.53.1402

Reference yield:

: 89-86-1
4-hydroxysalicylic acid

: 875544-25-5
2,4-diacetoxy-benzoic acid 2-phenylselanyl-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 4 h / 20 °C

2: SOCl₂ / CH₂Cl₂ / 3 h / Heating

3: dimethylaminopyridine; pyridine / CH₂Cl₂ / 3 h / 0 °C

With pyridine; dmap; thionyl chloride; In dichloromethane;
DOI:10.1248/cpb.53.1402

Reference yield:

: 1666-13-3
diphenyl diselenide

: 875544-25-5
2,4-diacetoxy-benzoic acid 2-phenylselanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaBH₄ / ethanol / 0 °C

1.2: 96 percent / ethanol / 3 h / Heating

2.1: dimethylaminopyridine; pyridine / CH₂Cl₂ / 3 h / 0 °C

With pyridine; dmap; sodium tetrahydroborate; In ethanol; dichloromethane;
DOI:10.1248/cpb.53.1402