4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(4-methylphenoxy)-

Base Information

Chemical Name:4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(4-methylphenoxy)-
CAS No.:137988-12-6
Molecular Formula:C₁₈H₁₄O₅
Molecular Weight:310.306
Hs Code.:
DSSTox Substance ID:DTXSID60160437
Wikidata:Q83028804
Mol file:137988-12-6.mol

Synonyms:BRN 5446815;4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(4-methylphenoxy)-;137988-12-6;7-(Acetyloxy)-3-(4-methylphenoxy)-4H-1-benzopyran-4-one;SCHEMBL18550844;DTXSID60160437;STL512862;AKOS030489084;3-(4-methylphenoxy)-7-acetoxychromone;4-oxo-3-(p-tolyloxy)-4H-chromen-7-yl acetate;3-(4-methylphenoxy)-4-oxo-4H-chromen-7-yl acetate

Suppliers and Price of 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(4-methylphenoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(4-methylphenoxy)-

Chemical Property:

Vapor Pressure:3.52E-08mmHg at 25°C
Boiling Point:446.9°Cat760mmHg
Flash Point:243°C
Density:1.301g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:310.08412354
Heavy Atom Count:23
Complexity:490

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)OC2=COC3=C(C2=O)C=CC(=C3)OC(=O)C

Technology Process of 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(4-methylphenoxy)-

There total 5 articles about 4H-1-Benzopyran-4-one, 7-(acetyloxy)-3-(4-methylphenoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 108-24-7
acetic anhydride

: 137987-96-3
7-Hydroxy-3-p-tolyloxy-chromen-4-one

: 137988-12-6
Acetic acid 4-oxo-3-p-tolyloxy-4H-chromen-7-yl ester

Guidance literature:: With pyridine;
DOI:10.1007/BF02291930

Reference yield:

: 33901-44-9
2-(4-methylphenoxy)acetonitrile

: 137988-12-6
Acetic acid 4-oxo-3-p-tolyloxy-4H-chromen-7-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) ZnCl₂, HCl gas, 2.) H₂O / 1.) benzene, overnight, 2.) boiling, 1 h

2: 94 percent / BF₃*Et₂O, PCl₅ / 50 - 60 °C

3: 96 percent / pyridine

With pyridine; hydrogenchloride; phosphorus pentachloride; boron trifluoride diethyl etherate; water; zinc(II) chloride;
DOI:10.1007/BF02291930

Reference yield:

: 137987-84-9
1-(2,4-dihydroxyphenyl)-2-(p-tolyloxy)ethanone

: 137988-12-6
Acetic acid 4-oxo-3-p-tolyloxy-4H-chromen-7-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / BF₃*Et₂O, PCl₅ / 50 - 60 °C

2: 96 percent / pyridine

With pyridine; phosphorus pentachloride; boron trifluoride diethyl etherate;
DOI:10.1007/BF02291930