2,2,6-Trimethylhept-5-enal

Base Information

Chemical Name:2,2,6-Trimethylhept-5-enal
CAS No.:52279-00-2
Molecular Formula:C10H18 O
Molecular Weight:154.252
Hs Code.:
European Community (EC) Number:257-809-9
UNII:EJ3S25TG9H
DSSTox Substance ID:DTXSID5068730
Nikkaji Number:J295.625J
Mol file:52279-00-2.mol

Synonyms:2,2,6-Trimethylhept-5-enal;5-Heptenal, 2,2,6-trimethyl-;52279-00-2;2,2,6-Trimethyl-5-heptenal;EINECS 257-809-9;EJ3S25TG9H;DTXSID5068730;EN300-1622166

Suppliers and Price of 2,2,6-Trimethylhept-5-enal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,2,6-Trimethylhept-5-enal

Chemical Property:

Vapor Pressure:0.279mmHg at 25°C
Boiling Point:203.3°C at 760 mmHg
Flash Point:71.6°C
PSA：17.07000
Density:0.836g/cm³
LogP:2.95790
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:154.135765193
Heavy Atom Count:11
Complexity:150

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CCCC(C)(C)C=O)C

Technology Process of 2,2,6-Trimethylhept-5-enal

There total 6 articles about 2,2,6-Trimethylhept-5-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 132462-50-1
2,2,6-trimethyl-5-hepten-1-ol

: 52279-00-2
2,2,6-trimethyl-hept-5-enal

Guidance literature:: With pyridinium chlorochromate; In diethyl ether; at 20 ℃; for 6h;
DOI:10.1021/ja012450c

Reference yield:

: 2270-59-9
1-bromo-4-methylpent-3-ene

: 52279-00-2
2,2,6-trimethyl-hept-5-enal

Guidance literature:: Multi-step reaction with 3 steps

1.1: di-iso-propylamine; n-butyllithium / tetrahydrofuran / 1 h / -78 °C

1.2: 74 percent / tetrahydrofuran / 10 h / 20 °C

2.1: 94 percent / LiAlH / diethyl ether / 4 h / 0 °C

3.1: 75 percent / PCC / diethyl ether / 6 h / 20 °C

With n-butyllithium; diisopropylamine; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja012450c

Reference yield:

: 132462-51-2
ethyl 2,2,6-trimethyl-hept-5-enoate

: 52279-00-2
2,2,6-trimethyl-hept-5-enal

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / LiAlH / diethyl ether / 4 h / 0 °C

2: 75 percent / PCC / diethyl ether / 6 h / 20 °C

With pyridinium chlorochromate; In diethyl ether;
DOI:10.1021/ja012450c