Pyridine, 2-[(2S,3E)-2-[[(1S)-1-(1,1-dimethylethyl)-1,2,3,4-tetrahydro-1-silanaphth alen-1-yl]oxy]-4-phenyl-3-butenyl]-

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Chemical Name:Pyridine, 2-[(2S,3E)-2-[[(1S)-1-(1,1-dimethylethyl)-1,2,3,4-tetrahydro-1-silanaphth alen-1-yl]oxy]-4-phenyl-3-butenyl]-
CAS No.:875796-55-7
Molecular Formula:C28H33NOSi
Molecular Weight:427.662
Hs Code.:

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Chemical Property of Pyridine, 2-[(2S,3E)-2-[[(1S)-1-(1,1-dimethylethyl)-1,2,3,4-tetrahydro-1-silanaphth alen-1-yl]oxy]-4-phenyl-3-butenyl]-

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Technology Process of Pyridine, 2-[(2S,3E)-2-[[(1S)-1-(1,1-dimethylethyl)-1,2,3,4-tetrahydro-1-silanaphth alen-1-yl]oxy]-4-phenyl-3-butenyl]-

There total 1 articles about Pyridine, 2-[(2S,3E)-2-[[(1S)-1-(1,1-dimethylethyl)-1,2,3,4-tetrahydro-1-silanaphth alen-1-yl]oxy]-4-phenyl-3-butenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 919513-39-6
(SiS)-1-tert-butyl-1,2,3,4-tetrahydro-1-silanaphthalene

: 106989-75-7
rac-(E)-4-phenyl-1-(pyridin-2-yl)but-3-en-2-ol

: (R,E)-4-phenyl-1-(pyridin-2-yl)but-3-en-2-ol

: 875796-55-7
(^SiS,S,E)-2-[2-(1-tert-butyl-1-silatetralinyl-1-oxy)-4-phenylbut-3-enyl]pyridine

Guidance literature:: With tris(3,5-dimethylphenyl)phosphine; copper(l) chloride; sodium t-butanolate; In toluene; at 20 ℃; for 24h; optical yield given as %ee; stereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.200801377