Carbamic acid, [(1S,2R)-2-hydroxy-3-[(2-hydroxy-5-methylphenyl)[(4-methoxyphenyl)sulf onyl]amino]-1-(phenylmethyl)propyl]-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Carbamic acid, [(1S,2R)-2-hydroxy-3-[(2-hydroxy-5-methylphenyl)[(4-methoxyphenyl)sulf onyl]amino]-1-(phenylmethyl)propyl]-, 1,1-dimethylethyl ester
• CAS No.: 875932-82-4
• Molecular Formula: C₂₉H₃₆N₂O₇S
• Molecular Weight: 556.68

Synonyms:

Chemical Property of Carbamic acid, [(1S,2R)-2-hydroxy-3-[(2-hydroxy-5-methylphenyl)[(4-methoxyphenyl)sulf onyl]amino]-1-(phenylmethyl)propyl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of Carbamic acid, [(1S,2R)-2-hydroxy-3-[(2-hydroxy-5-methylphenyl)[(4-methoxyphenyl)sulf onyl]amino]-1-(phenylmethyl)propyl]-, 1,1-dimethylethyl ester

There total 2 articles about Carbamic acid, [(1S,2R)-2-hydroxy-3-[(2-hydroxy-5-methylphenyl)[(4-methoxyphenyl)sulf onyl]amino]-1-(phenylmethyl)propyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1-oxiranyl-2-phenylethyl)carbamic acid tert-butyl ester (98760-08-8,98818-34-9,98818-35-0,103127-56-6,98737-29-2) → {(1S,2R)-1-Benzyl-2-hydroxy-3-[(2-hydroxy-5-methyl-phenyl)-(4-methoxy-benzenesulfonyl)-amino]-propyl}-carbamic acid tert-butyl ester (875932-82-4)

Guidance literature:

Multi-step reaction with 2 steps

1: propan-2-ol / 60 °C

2: pyridine / acetonitrile / 20 °C

With pyridine; In isopropyl alcohol; acetonitrile;

DOI:10.1016/j.bmc.2005.09.026

Reference yield:

3-amino-4-hydroxytoluene (95-84-1) → {(1S,2R)-1-Benzyl-2-hydroxy-3-[(2-hydroxy-5-methyl-phenyl)-(4-methoxy-benzenesulfonyl)-amino]-propyl}-carbamic acid tert-butyl ester (875932-82-4)

Guidance literature:

Multi-step reaction with 2 steps

1: propan-2-ol / 60 °C

2: pyridine / acetonitrile / 20 °C

With pyridine; In isopropyl alcohol; acetonitrile;

DOI:10.1016/j.bmc.2005.09.026

Reference yield:

{(1S,2R)-1-Benzyl-2-hydroxy-3-[(2-hydroxy-5-methyl-phenyl)-(4-methoxy-benzenesulfonyl)-amino]-propyl}-carbamic acid tert-butyl ester (875932-82-4) → N-(3-amino-2-hydroxy-4-phenyl-butyl)-N-(2-hydroxy-5-methyl-phenyl)-4-methoxy-benzenesulfonamide

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.bmc.2005.09.026

upstream raw materials:

(1-oxiranyl-2-phenylethyl)carbamic acid tert-butyl ester

3-amino-4-hydroxytoluene

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