2-Pyridinecarboxamide, 6,6'-[methylenebis(1-ethyl-1H-benzimidazole-5,2-diyl)]bis[N-ethyl-N-[4-[ [4-(ethylamino)-3-nitrophenyl]methyl]-2-nitrophenyl]-

Base Information

Chemical Name:2-Pyridinecarboxamide, 6,6'-[methylenebis(1-ethyl-1H-benzimidazole-5,2-diyl)]bis[N-ethyl-N-[4-[ [4-(ethylamino)-3-nitrophenyl]methyl]-2-nitrophenyl]-
CAS No.:876017-86-6
Molecular Formula:C65H62N14O10
Molecular Weight:1199.3
Hs Code.:

2-Pyridinecarboxamide,
6,6'-[methylenebis(1-ethyl-1H-benzimidazole-5,2-diyl)]bis[N-ethyl-N-[4-[
[4-(ethylamino)-3-nitrophenyl]methyl]-2-nitrophenyl]-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Pyridinecarboxamide, 6,6'-[methylenebis(1-ethyl-1H-benzimidazole-5,2-diyl)]bis[N-ethyl-N-[4-[ [4-(ethylamino)-3-nitrophenyl]methyl]-2-nitrophenyl]-

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Technology Process of 2-Pyridinecarboxamide, 6,6'-[methylenebis(1-ethyl-1H-benzimidazole-5,2-diyl)]bis[N-ethyl-N-[4-[ [4-(ethylamino)-3-nitrophenyl]methyl]-2-nitrophenyl]-

There total 2 articles about 2-Pyridinecarboxamide, 6,6'-[methylenebis(1-ethyl-1H-benzimidazole-5,2-diyl)]bis[N-ethyl-N-[4-[ [4-(ethylamino)-3-nitrophenyl]methyl]-2-nitrophenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 218461-49-5
bis(1-ethyl-2-[(6'-carboxy)pyridin-2'-yl]benzimidazol-5-yl)-methane

: 876017-86-6
C₆₅H₆₂N₁₄O₁₀

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; DMF / CH₂Cl₂ / 3 h / Heating

2: 1.49 g / ethyldiisopropylamine / CH₂Cl₂ / 12 h / Heating

With thionyl chloride; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/anie.200503040

Reference yield:

: C₃₁H₂₄Cl₂N₆O₂

: 101588-67-4
3,3′-dinitro-4,4′-di(N-ethylamino)diphenylmethane

: 876017-86-6
C₆₅H₆₂N₁₄O₁₀

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 12h; Heating;
DOI:10.1002/anie.200503040

Reference yield:

: 876017-86-6
C₆₅H₆₂N₁₄O₁₀

: 179469-06-8
2-(hydroxycarbonyl)-6-[(N,N-diethylamino)carbonyl]pyridine

: C₈₇H₈₆N₁₈O₁₄

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; 1,2-dichloro-ethane; for 12h; Heating;
DOI:10.1002/anie.200503040