5-(4-Fluorobenzyl)-2,2-diMethyl-1,3dioxane-4,6-dione

Base Information

Chemical Name:5-(4-Fluorobenzyl)-2,2-diMethyl-1,3dioxane-4,6-dione
CAS No.:876405-68-4
Molecular Formula:C13H13FO4
Molecular Weight:252.242
Hs Code.:
Mol file:876405-68-4.mol

Synonyms:5-(4-Fluoro-benzyl)-2,2-dimethyl-[1,3]dioxane-4,6-dione;5-(4-fluorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione;2,2-Dimethyl-5-(4-fluorophenyl)methyl-1,3-dioxane-4,6-dione;

Suppliers and Price of 5-(4-Fluorobenzyl)-2,2-diMethyl-1,3dioxane-4,6-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5-(4-FLUOROBENZYL)-2,2-DIMETHYL-1,3DIOXANE-4,6-DIONE 95.00%
5MG
$ 500.53

Total 3 raw suppliers

Chemical Property of 5-(4-Fluorobenzyl)-2,2-diMethyl-1,3dioxane-4,6-dione

Chemical Property:

Melting Point:96 - 98 °C
Boiling Point:449.5±35.0 °C(Predicted)
PKA:12.44±0.40(Predicted)
PSA：52.60000
Density:1.245±0.06 g/cm3(Predicted)
LogP:1.82050

Purity/Quality:

98%min ^*data from raw suppliers

5-(4-FLUOROBENZYL)-2,2-DIMETHYL-1,3DIOXANE-4,6-DIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(4-Fluorobenzyl)-2,2-diMethyl-1,3dioxane-4,6-dione

There total 19 articles about 5-(4-Fluorobenzyl)-2,2-diMethyl-1,3dioxane-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 5-(4-octyloxybenzyl)-5-(4-fluorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

: 876405-68-4
5-(4-fluorobenzyl)-2,2-dimethyl-[1,3]dioxane-4,6-dione

: 67698-82-2
1-methyl-4-(octyloxy)benzene

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 65 ℃; for 24h; under 760.051 Torr; Sealed tube;
DOI:10.1002/adsc.201600535

Reference yield:

: 2033-24-1
cycl-isopropylidene malonate

: 459-57-4
4-fluorobenzaldehyde

: 876405-68-4
5-(4-fluorobenzyl)-2,2-dimethyl-[1,3]dioxane-4,6-dione

Guidance literature:: With 2,6-dimethyl-1,4-dihydropyrimidine-3,5-dicarboxylic acid diethyl ester; L-proline; In acetonitrile; at 25 ℃; for 3h;
DOI:10.1016/j.tetlet.2005.11.128