4-[7-(5-hydroxy-2-methyl-5,5-diphenyl-pentan-2-yl)-4,8-dithia-2,6-diazabicyclo[3.3.0]octa-2,6,9-trien-3-yl]-4-methyl-1,1-diphenyl-pentan-1-ol

Base Information

• Chemical Name: 4-[7-(5-hydroxy-2-methyl-5,5-diphenyl-pentan-2-yl)-4,8-dithia-2,6-diazabicyclo[3.3.0]octa-2,6,9-trien-3-yl]-4-methyl-1,1-diphenyl-pentan-1-ol
• CAS No.: 33328-48-2
• Molecular Formula: C₄₀H₄₂N₂O₂S₂
• Molecular Weight: 646.918

Synonyms:

Chemical Property of 4-[7-(5-hydroxy-2-methyl-5,5-diphenyl-pentan-2-yl)-4,8-dithia-2,6-diazabicyclo[3.3.0]octa-2,6,9-trien-3-yl]-4-methyl-1,1-diphenyl-pentan-1-ol

Chemical Property:

• Boiling Point: 781.1°Cat760mmHg
• Flash Point: 426.2°C
• Density: 1.214g/cm³

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 4-[7-(5-hydroxy-2-methyl-5,5-diphenyl-pentan-2-yl)-4,8-dithia-2,6-diazabicyclo[3.3.0]octa-2,6,9-trien-3-yl]-4-methyl-1,1-diphenyl-pentan-1-ol

There total 3 articles about 4-[7-(5-hydroxy-2-methyl-5,5-diphenyl-pentan-2-yl)-4,8-dithia-2,6-diazabicyclo[3.3.0]octa-2,6,9-trien-3-yl]-4-methyl-1,1-diphenyl-pentan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-dimethyl-4,4'-thiazolo[5,4-d]thiazole-2,5-diyl-bis-pentanenitrile (32563-71-6) → 4,4'-dimethyl-1,1,1',1'-tetraphenyl-4,4'-thiazolo[5,4-d]thiazole-2,5-diyl-bis-pentan-1-ol (33328-48-2)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NaOH / ethanol

2: aq. HCl

3: benzene; diethyl ether

With hydrogenchloride; sodium hydroxide; In diethyl ether; ethanol; benzene;

DOI:10.1021/jm00290a018

Reference yield:

4,4'-dimethyl-4,4'-thiazolo[5,4-d]thiazole-2,5-diyl-bis-pentanoic acid (33311-49-8) → 4,4'-dimethyl-1,1,1',1'-tetraphenyl-4,4'-thiazolo[5,4-d]thiazole-2,5-diyl-bis-pentan-1-ol (33328-48-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl

2: benzene; diethyl ether

With hydrogenchloride; In diethyl ether; benzene;

DOI:10.1021/jm00290a018

Reference yield:

Dimethyl-γ,γ,γ',γ'-Tetramethylthiazolo<5,4-d>-thiazol-2,5-dibutyrat + phenylmagnesium bromide → 4,4'-dimethyl-1,1,1',1'-tetraphenyl-4,4'-thiazolo[5,4-d]thiazole-2,5-diyl-bis-pentan-1-ol (33328-48-2)

Guidance literature:

In diethyl ether; benzene;

DOI:10.1021/jm00290a018

upstream raw materials:

4,4'-dimethyl-4,4'-thiazolo[5,4-d]thiazole-2,5-diyl-bis-pentanenitrile

4,4'-dimethyl-4,4'-thiazolo[5,4-d]thiazole-2,5-diyl-bis-pentanoic acid

Downstream raw materials:

2,5-bis-(1,1-dimethyl-4,4-diphenyl-but-3-enyl)-thiazolo[5,4-d]thiazole

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