dichloropalladium - dicyclohexylphosphane (1:2)

Base Information

Chemical Name:dichloropalladium - dicyclohexylphosphane (1:2)
CAS No.:64659-74-1
Molecular Formula:C₂₄H₄₆Cl₂P₂Pd
Molecular Weight:573.903
Hs Code.:

Synonyms:Phosphine,dicyclohexyl-, palladium complex; NSC 236263;cis-Bis(dicyclohexylphosphine)dichloropalladium;cis-Dichlorobis(dicyclohexylphosphine)palladium

Suppliers and Price of dichloropalladium - dicyclohexylphosphane (1:2)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of dichloropalladium - dicyclohexylphosphane (1:2)

Chemical Property:

Vapor Pressure:0.00373mmHg at 25°C
Boiling Point:289.8°Cat760mmHg
Flash Point:129.1°C
Density:g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of dichloropalladium - dicyclohexylphosphane (1:2)

There total 1 articles about dichloropalladium - dicyclohexylphosphane (1:2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 829-84-5
dicyclohexylphosphane

: 155898-37-6,64659-74-1
[PdCl₂(HP(C₆H₁₁)2)2]

Guidance literature:: In toluene; (N2); room temp.;
DOI:10.1039/a607334d

Reference yield: 64.0%

: 64659-74-1,155898-37-6
PdCl₂(P(C₆H₁₁)2H)2

: (Pd(P(C₆H₁₁)2)(Cl)(P(C₆H₁₁)2H))2

Guidance literature:: With PhONa; In toluene; byproducts: NaCl, C6H5OH; PhONa is added to a suspension of (PdCl2(PCy2H)2) in toluene under nitrogen, stirred 3 h at ambient temp.; solvent is evapd., residue is extd. (CHCl3), concd., pptd. (acetone), filtn., drying (vac.); elem. anal.;

Reference yield: 46.0%

: 64659-74-1,155898-37-6
PdCl₂(P(C₆H₁₁)2H)2

: 139-02-6
sodium phenoxide

: C₆₀H₉₈O₂P₄Pd₂

Guidance literature:: In toluene; byproducts: NaCl, H2, C6H5OH; suspension of (PdCl2(PCy2H)2) and PhONa in toluene is stirred 3 h at 50°C under nitrogen, suspension is left overnight at ambient temp.; filtn., concn., acetone is added, pptn., filtn., drying (vac.); elem. nal.;