5H-1,3-Dithiolo[4,5-c]pyrrole, 5-[[3,5-bis(1,1-dimethylethyl)phenyl]methyl]-2-[4-(ethylthio)-5-[[2-(2-meth oxyethoxy)ethyl]thio]-1,3-dithiol-2-ylidene]-

Base Information

Chemical Name:5H-1,3-Dithiolo[4,5-c]pyrrole, 5-[[3,5-bis(1,1-dimethylethyl)phenyl]methyl]-2-[4-(ethylthio)-5-[[2-(2-meth oxyethoxy)ethyl]thio]-1,3-dithiol-2-ylidene]-
CAS No.:877032-14-9
Molecular Formula:C30H41NO2S6
Molecular Weight:640.057
Hs Code.:

5H-1,3-Dithiolo[4,5-c]pyrrole,
5-[[3,5-bis(1,1-dimethylethyl)phenyl]methyl]-2-[4-(ethylthio)-5-[[2-(2-meth
oxyethoxy)ethyl]thio]-1,3-dithiol-2-ylidene]-

Synonyms:

Suppliers and Price of 5H-1,3-Dithiolo[4,5-c]pyrrole, 5-[[3,5-bis(1,1-dimethylethyl)phenyl]methyl]-2-[4-(ethylthio)-5-[[2-(2-meth oxyethoxy)ethyl]thio]-1,3-dithiol-2-ylidene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5H-1,3-Dithiolo[4,5-c]pyrrole, 5-[[3,5-bis(1,1-dimethylethyl)phenyl]methyl]-2-[4-(ethylthio)-5-[[2-(2-meth oxyethoxy)ethyl]thio]-1,3-dithiol-2-ylidene]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5H-1,3-Dithiolo[4,5-c]pyrrole, 5-[[3,5-bis(1,1-dimethylethyl)phenyl]methyl]-2-[4-(ethylthio)-5-[[2-(2-meth oxyethoxy)ethyl]thio]-1,3-dithiol-2-ylidene]-

There total 4 articles about 5H-1,3-Dithiolo[4,5-c]pyrrole, 5-[[3,5-bis(1,1-dimethylethyl)phenyl]methyl]-2-[4-(ethylthio)-5-[[2-(2-meth oxyethoxy)ethyl]thio]-1,3-dithiol-2-ylidene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 877032-13-8
2-{4-(2-(2-Methoxyethoxy)-ethylthio)-5-ethylthio-1,3-dithiol-2-ylidene}-(1,3)-dithiolo[4,5-c]pyrrole

: 62938-08-3
3,5-di-tert-butylbenzyl bromide

: 877032-14-9
5-(3,5-di-tert-butyl-benzyl)-2-{4-ethylsulfanyl-5-[2-(2-methoxy-ethoxy)-ethylsulfanyl]-[1,3]dithiol-2-ylidene}-5H-[1,3]dithiolo[4,5-c]pyrrole

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1039/b511575b

Reference yield:

: 846571-61-7
N-tosyl-2-[4-(ethylthio)-5-(2-cyanoethylthio)-(1,3)-dithiole-2-ylidene]-(1,3)-dithiolo[4,5-c]pyrrole

: 877032-14-9
5-(3,5-di-tert-butyl-benzyl)-2-{4-ethylsulfanyl-5-[2-(2-methoxy-ethoxy)-ethylsulfanyl]-[1,3]dithiol-2-ylidene}-5H-[1,3]dithiolo[4,5-c]pyrrole

Guidance literature:: Multi-step reaction with 4 steps

1: CsOH*H₂O / methanol; tetrahydrofuran / 20 °C

2: 0.49 g / methanol; tetrahydrofuran / 4 h / 20 °C

3: 93 percent / NaOMe / methanol; tetrahydrofuran / 0.5 h / Heating

4: 92 percent / NaH / dimethylformamide / 1 h / 20 °C

With cesium hydroxide; sodium methylate; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/b511575b

Reference yield:

: 877032-12-7
C₂₂H₂₅NO₄S₇

: 877032-14-9
5-(3,5-di-tert-butyl-benzyl)-2-{4-ethylsulfanyl-5-[2-(2-methoxy-ethoxy)-ethylsulfanyl]-[1,3]dithiol-2-ylidene}-5H-[1,3]dithiolo[4,5-c]pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaOMe / methanol; tetrahydrofuran / 0.5 h / Heating

2: 92 percent / NaH / dimethylformamide / 1 h / 20 °C

With sodium methylate; sodium hydride; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1039/b511575b