2-Butenoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-, methyl ester

Base Information

Chemical Name:2-Butenoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-, methyl ester
CAS No.:877055-57-7
Molecular Formula:C32H42N4O8
Molecular Weight:610.707
Hs Code.:

2-Butenoic acid,
4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4
-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-,
methyl ester

Synonyms:

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Chemical Property of 2-Butenoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-, methyl ester

Chemical Property:

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Safty Information:

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Useful:

Technology Process of 2-Butenoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-, methyl ester

There total 2 articles about 2-Butenoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 877055-56-6
(4-{3-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-2-oxo-propylcarbamoyl}-benzyl)-carbamic acid tert-butyl ester

: 1067-74-9
Methyl diethylphosphonoacetate

: 4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylimino]-methyl}-butyric acid methyl ester

: 877055-57-7
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-but-2-enoic acid methyl ester

Guidance literature:: Methyl diethylphosphonoacetate; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 20 ℃; for 0.25h;

(4-{3-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-2-oxo-propylcarbamoyl}-benzyl)-carbamic acid tert-butyl ester; In tetrahydrofuran; toluene; at 0 ℃; for 2.5h;
DOI:10.1002/chem.200500901

Reference yield:

: 33233-67-9
4-(tert-Butoxycarbonylaminomethyl)benzoic acid

: 877055-57-7
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-but-2-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 79 percent / ethyldiisopropylamine; HBTU / dimethylformamide / 20 °C

2.1: potassium bis(trimethylsilyl)amide / toluene; tetrahydrofuran / 0.25 h / 20 °C

2.2: 40 percent / toluene; tetrahydrofuran / 2.5 h / 0 °C

With potassium hexamethylsilazane; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.200500901