Butanoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-, methyl ester

Base Information

Chemical Name:Butanoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-, methyl ester
CAS No.:877055-58-8
Molecular Formula:C32H44N4O8
Molecular Weight:612.723
Hs Code.:

Butanoic acid,
4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4
-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-,
methyl ester

Synonyms:

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Chemical Property of Butanoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-, methyl ester

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Technology Process of Butanoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-, methyl ester

There total 3 articles about Butanoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 877055-57-7
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-but-2-enoic acid methyl ester

: 877055-58-8
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-butyric acid methyl ester

Guidance literature:: With ammonium formate; palladium on activated charcoal; at 20 ℃; for 16h;
DOI:10.1002/chem.200500901

Reference yield:

: 877055-56-6
(4-{3-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-2-oxo-propylcarbamoyl}-benzyl)-carbamic acid tert-butyl ester

: 877055-58-8
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium bis(trimethylsilyl)amide / toluene; tetrahydrofuran / 0.25 h / 20 °C

1.2: 40 percent / toluene; tetrahydrofuran / 2.5 h / 0 °C

2.1: 86 percent / ammonium formate / Pd/C / 16 h / 20 °C

With ammonium formate; potassium hexamethylsilazane; palladium on activated charcoal; In tetrahydrofuran; toluene;
DOI:10.1002/chem.200500901

Reference yield:

: 33233-67-9
4-(tert-Butoxycarbonylaminomethyl)benzoic acid

: 877055-58-8
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 79 percent / ethyldiisopropylamine; HBTU / dimethylformamide / 20 °C

2.1: potassium bis(trimethylsilyl)amide / toluene; tetrahydrofuran / 0.25 h / 20 °C

2.2: 40 percent / toluene; tetrahydrofuran / 2.5 h / 0 °C

3.1: 86 percent / ammonium formate / Pd/C / 16 h / 20 °C

With ammonium formate; potassium hexamethylsilazane; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.200500901