Butanoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-

Base Information

Chemical Name:Butanoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-
CAS No.:877055-59-9
Molecular Formula:C31H42N4O8
Molecular Weight:598.696
Hs Code.:

Butanoic acid,
4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4
-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-

Synonyms:

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Chemical Property of Butanoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-

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Technology Process of Butanoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]-

There total 4 articles about Butanoic acid, 4-[[4-[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]-3-[[[4 -[[[(1,1-dimethylethoxy)carbonyl]amino]methyl]benzoyl]amino]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 877055-58-8
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-butyric acid methyl ester

: 877055-59-9
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-butyric acid

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; at 20 ℃; for 16h;
DOI:10.1002/chem.200500901

Reference yield:

: 877055-56-6
(4-{3-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-2-oxo-propylcarbamoyl}-benzyl)-carbamic acid tert-butyl ester

: 877055-59-9
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium bis(trimethylsilyl)amide / toluene; tetrahydrofuran / 0.25 h / 20 °C

1.2: 40 percent / toluene; tetrahydrofuran / 2.5 h / 0 °C

2.1: 86 percent / ammonium formate / Pd/C / 16 h / 20 °C

3.1: 83 percent / aq. NaOH / dioxane / 16 h / 20 °C

With sodium hydroxide; ammonium formate; potassium hexamethylsilazane; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; toluene;
DOI:10.1002/chem.200500901

Reference yield:

: 877055-57-7
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-but-2-enoic acid methyl ester

: 877055-59-9
4-[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-3-{[4-(tert-butoxycarbonylamino-methyl)-benzoylamino]-methyl}-butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / ammonium formate / Pd/C / 16 h / 20 °C

2: 83 percent / aq. NaOH / dioxane / 16 h / 20 °C

With sodium hydroxide; ammonium formate; palladium on activated charcoal; In 1,4-dioxane;
DOI:10.1002/chem.200500901