2-(Chloromethyl)-1,4-dioxaspiro[4.5]decane

Base Information

• Chemical Name: 2-(Chloromethyl)-1,4-dioxaspiro[4.5]decane
• CAS No.: 5503-32-2
• Molecular Formula: C9H15ClO2
• Molecular Weight: 190.67
• Hs Code.: 2932999099
• NSC Number: 45315,41991
• Nikkaji Number: J2.091.702D
• Mol file: 5503-32-2.mol

Synonyms:2-(Chloromethyl)-1,4-dioxaspiro[4.5]decane;5503-32-2;3-(chloromethyl)-1,4-dioxaspiro[4.5]decane;1, 2-(chloromethyl)-;2-(Chloromethyl)-1,4-dioxaspiro(4.5)decane;NSC 45315;NSC 41991;AI3-31959;AI 3-31959;SCHEMBL6218973;1,4-Dioxaspiro(4.5)decane, 2-(chloromethyl)- (8CI)(9CI);NSC41991;NSC45315;NSC-41991;NSC-45315;AKOS015899027;1-chloro-2,3-O-cyclohexylidenepropane;SB46403;SB48100;CS-0453519;FT-0696711;FT-0696712;FT-0738219;EN300-373456;1,4-Dioxaspiro(4.5)decane, 2-(chloromethyl)-

Chemical Property of 2-(Chloromethyl)-1,4-dioxaspiro[4.5]decane

Chemical Property:

• Vapor Pressure: 0.0101mmHg at 25°C
• Boiling Point: 272.4°Cat760mmHg
• Flash Point: 105.8°C
• PSA: 18.46000
• Density: 1.15g/cm³
• LogP: 2.30100
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 190.0760574
• Heavy Atom Count: 12
• Complexity: 155

Purity/Quality:

99% ^*data from raw suppliers

2-(Chloromethyl)-1,4-dioxaspiro[4.5]decane 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1CCC2(CC1)OCC(O2)CCl

Technology Process of 2-(Chloromethyl)-1,4-dioxaspiro[4.5]decane

There total 3 articles about 2-(Chloromethyl)-1,4-dioxaspiro[4.5]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + 3-monochloro-1,2-propanediol (96-24-2) → 2-1,4-dioxaspiro<4,5>decane (5503-32-2,1098589-87-7)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; Heating;

DOI:10.1021/jm021078o

Reference yield: 98.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + epichlorohydrin (106-89-8,24969-06-0,13403-37-7) → 2-1,4-dioxaspiro<4,5>decane (5503-32-2,1098589-87-7)

Guidance literature:

tetrafluoroboric acid; In water; at 100 ℃; for 2.5h;

DOI:10.1007/BF00633210

Reference yield:

→ 2-1,4-dioxaspiro<4,5>decane (5503-32-2,1098589-87-7)

Guidance literature:

upstream raw materials:

cyclohexanone

epichlorohydrin

3-monochloro-1,2-propanediol

Downstream raw materials:

2-Benzylsulfanylmethyl-1,4-dioxa-spiro[4.5]decane

2-Phenylsulfanylmethyl-1,4-dioxa-spiro[4.5]decane

cyclohexanone

3-monochloro-1,2-propanediol