L-Phenylalanine, N-[2-[(acetylthio)methyl]-1-oxo-3-phenylpropyl]-4-[[(4R)-4-amino-5-[(2S) -2-cyano-1-pyrrolidinyl]-1,5-dioxopentyl]amino]-, methyl ester

Base Information

• Chemical Name: L-Phenylalanine, N-[2-[(acetylthio)methyl]-1-oxo-3-phenylpropyl]-4-[[(4R)-4-amino-5-[(2S) -2-cyano-1-pyrrolidinyl]-1,5-dioxopentyl]amino]-, methyl ester
• CAS No.: 877374-23-7
• Molecular Formula: C32H39N5O6S
• Molecular Weight: 621.758

Synonyms:

Chemical Property of L-Phenylalanine, N-[2-[(acetylthio)methyl]-1-oxo-3-phenylpropyl]-4-[[(4R)-4-amino-5-[(2S) -2-cyano-1-pyrrolidinyl]-1,5-dioxopentyl]amino]-, methyl ester

Chemical Property:

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Useful:

Technology Process of L-Phenylalanine, N-[2-[(acetylthio)methyl]-1-oxo-3-phenylpropyl]-4-[[(4R)-4-amino-5-[(2S) -2-cyano-1-pyrrolidinyl]-1,5-dioxopentyl]amino]-, methyl ester

There total 1 articles about L-Phenylalanine, N-[2-[(acetylthio)methyl]-1-oxo-3-phenylpropyl]-4-[[(4R)-4-amino-5-[(2S) -2-cyano-1-pyrrolidinyl]-1,5-dioxopentyl]amino]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-acetylsulfanylmethyl-3-phenylpropionylamino)-3-{4-[4-tert-butoxycarbonylamino-5-(2-cyanopyrrolidin-1-yl)-5-oxopentanoylamino]-phenyl}-propionic acid methyl ester (877374-22-6) → 2-(2-acetylsulfanylmethyl-3-phenylpropionylamino)-3-{4-[4-amino-5-(2-cyanopyrrolidin-1-yl)-5-oxopentanoylamino]-phenyl}-propionic acid methyl ester (877374-23-7)

Guidance literature:

With trifluoroacetic acid; In water; at 20 ℃; for 4h;

Reference yield:

2-(2-acetylsulfanylmethyl-3-phenylpropionylamino)-3-{4-[4-amino-5-(2-cyanopyrrolidin-1-yl)-5-oxopentanoylamino]-phenyl}-propionic acid methyl ester (877374-23-7) → 3-{4-[4-amino-5-(2-cyanopyrrolidin-1-yl)-5-oxopentanoylamino]-phenyl}-2-(2-mercaptomethyl-3-phenylpropionylamino)-propionic acid (877373-91-6)

Guidance literature:

With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 6h;

upstream raw materials:

2-(2-acetylsulfanylmethyl-3-phenylpropionylamino)-3-{4-[4-tert-butoxycarbonylamino-5-(2-cyanopyrrolidin-1-yl)-5-oxopentanoylamino]-phenyl}-propionic acid methyl ester

Downstream raw materials:

3-{4-[4-amino-5-(2-cyanopyrrolidin-1-yl)-5-oxopentanoylamino]-phenyl}-2-(2-mercaptomethyl-3-phenylpropionylamino)-propionic acid

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