Carbamic acid, [[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-[4-( 2-pyridinyl)-1-piperidinyl]-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-[4-( 2-pyridinyl)-1-piperidinyl]-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl ester
CAS No.:877678-72-3
Molecular Formula:C31H45ClN6O3Si
Molecular Weight:613.275
Hs Code.:

Carbamic acid,
[[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-[4-(
2-pyridinyl)-1-piperidinyl]-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl
ester

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Chemical Property of Carbamic acid, [[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-[4-( 2-pyridinyl)-1-piperidinyl]-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl ester

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Technology Process of Carbamic acid, [[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-[4-( 2-pyridinyl)-1-piperidinyl]-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl ester

There total 1 articles about Carbamic acid, [[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-[4-( 2-pyridinyl)-1-piperidinyl]-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: N-[2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-chlorophenyl]-4-pyridin-2-ylpiperidine-1-carbimidothioic acid

: 6926-09-6
(tert-butoxycarbonyl)glycine hydrazide

: 877678-72-3
tert-butyl {4-[2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-chlorophenyl]-5-(4-pyridin-2-ylpiperidin-1-yl)-4H-1,2,4-triazol-3-yl}

Guidance literature:: N-[2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-chlorophenyl]-4-pyridin-2-ylpiperidine-1-carbimidothioic acid; (tert-butoxycarbonyl)glycine hydrazide; trifluoroacetic acid; In tetrahydrofuran; for 24h; Heating / reflux;

With ammonia; In tetrahydrofuran; water;

Reference yield: 80.0%

: 877678-72-3
tert-butyl {4-[2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-chlorophenyl]-5-(4-pyridin-2-ylpiperidin-1-yl)-4H-1,2,4-triazol-3-yl}

: 877678-73-4
tert-butyl {[4-[4-chloro-2-(hydroxymethyl)phenyl]-5-(4-pyridin-2-ylpiperidiri-1-yl)-4H-1,2,4-triazol-3-y I]methyl}carbamate

Guidance literature:: tert-butyl {4-[2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-chlorophenyl]-5-(4-pyridin-2-ylpiperidin-1-yl)-4H-1,2,4-triazol-3-yl}; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.666667h;

With sodium hydrogencarbonate; In tetrahydrofuran; water; for 0.5h;