Carbamic acid, [[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-(4- phenyl-1-piperidinyl)-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-(4- phenyl-1-piperidinyl)-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl ester
CAS No.:877678-80-3
Molecular Formula:C32H46ClN5O3Si
Molecular Weight:612.287
Hs Code.:

Carbamic acid,
[[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-(4-
phenyl-1-piperidinyl)-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl
ester

Synonyms:

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Chemical Property of Carbamic acid, [[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-(4- phenyl-1-piperidinyl)-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl ester

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Technology Process of Carbamic acid, [[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-(4- phenyl-1-piperidinyl)-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl ester

There total 3 articles about Carbamic acid, [[4-[4-chloro-2-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]phenyl]-5-(4- phenyl-1-piperidinyl)-4H-1,2,4-triazol-3-yl]methyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 877678-76-7
C₂₆H₃₇ClN₂OSSi

: 6926-09-6
(tert-butoxycarbonyl)glycine hydrazide

: 877678-80-3
tert-butyl {[4-[2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-chlorophenyl]-5-(4-phenylpiperidin-1-yl)-4H-1,2,'4-triazol-3-yl]methyl}carbamate

Guidance literature:: With trifluoroacetic acid; In tetrahydrofuran; for 22h; Reflux;
DOI:10.1055/s-2008-1078208

Reference yield: 34.0%

: N-[2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-chlorophenyl]-4-phenylpiperidine-1-carbimidothioic acid

: 6926-09-6
(tert-butoxycarbonyl)glycine hydrazide

: 877678-81-4
tert-butyl {[4-[4-chloro-2-(hydroxymethyl)phenyl]-5-(4-phenylpiperidin-1-yl)-4H-1,2,4-triazol-3-yl]methyl}carbamate

: 877678-80-3
tert-butyl {[4-[2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-chlorophenyl]-5-(4-phenylpiperidin-1-yl)-4H-1,2,'4-triazol-3-yl]methyl}carbamate

Guidance literature:: N-[2-({[tert-butyl(dimethyl)silyl]oxy}methyl)-4-chlorophenyl]-4-phenylpiperidine-1-carbimidothioic acid; (tert-butoxycarbonyl)glycine hydrazide; trifluoroacetic acid; In tetrahydrofuran; for 16h; Heating / reflux;

With ammonia; In tetrahydrofuran; water; at 20 ℃;