Cyclohexanol, 4-methyl-4-[(4-nitrophenoxy)methyl]-, cis-

Base Information

Chemical Name:Cyclohexanol, 4-methyl-4-[(4-nitrophenoxy)methyl]-, cis-
CAS No.:87787-14-2
Molecular Formula:C14H19NO4
Molecular Weight:265.309
Hs Code.:

Synonyms:

Suppliers and Price of Cyclohexanol, 4-methyl-4-[(4-nitrophenoxy)methyl]-, cis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Cyclohexanol, 4-methyl-4-[(4-nitrophenoxy)methyl]-, cis-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclohexanol, 4-methyl-4-[(4-nitrophenoxy)methyl]-, cis-

There total 7 articles about Cyclohexanol, 4-methyl-4-[(4-nitrophenoxy)methyl]-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1523-89-3
methyl 1-methyl-4-oxo-2-cyclohexene-1-carboxylate

: 87787-14-2
4-(c-4-hydroxy-1-methyl-r-1-cyclohexylmethoxy)nitrobenzene

Guidance literature:: Multi-step reaction with 7 steps

1: 95.4 percent / H₂ / Pd-C (50percent wet) / ethyl acetate / 760 Torr

2: 1.) H₂; 2.) 2N KOH / 1.) PtO₂ / 1.) AcOH, RT, 1 atm; 2.) MeOH, reflux, 1 h

3: diethyl ether

4: p-TsOH / diethyl ether / 2 h / Ambient temperature

5: 76.9 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

6: NaH / dimethylsulfoxide / 3 h / 30 °C

7: 2N HCl / methanol / 1 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; hydrogen; sodium hydride; toluene-4-sulfonic acid; platinum(IV) oxide; palladium on activated charcoal; In methanol; diethyl ether; dimethyl sulfoxide; ethyl acetate;
DOI:10.1248/cpb.32.2267

Reference yield:

: 37480-41-4
methyl 1-methyl-4-oxo-1-cyclohexanecarboxylate

: 87787-14-2
4-(c-4-hydroxy-1-methyl-r-1-cyclohexylmethoxy)nitrobenzene

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) H₂; 2.) 2N KOH / 1.) PtO₂ / 1.) AcOH, RT, 1 atm; 2.) MeOH, reflux, 1 h

2: diethyl ether

3: p-TsOH / diethyl ether / 2 h / Ambient temperature

4: 76.9 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

5: NaH / dimethylsulfoxide / 3 h / 30 °C

6: 2N HCl / methanol / 1 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; hydrogen; sodium hydride; toluene-4-sulfonic acid; platinum(IV) oxide; In methanol; diethyl ether; dimethyl sulfoxide;
DOI:10.1248/cpb.32.2267