Benzenesulfonamide, N-[(1R,2S)-2-hydroxy-1-phenylpropyl]-4-methyl-

Base Information

Chemical Name:Benzenesulfonamide, N-[(1R,2S)-2-hydroxy-1-phenylpropyl]-4-methyl-
CAS No.:877994-35-9
Molecular Formula:C16H19NO3S
Molecular Weight:305.398
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonamide, N-[(1R,2S)-2-hydroxy-1-phenylpropyl]-4-methyl-

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzenesulfonamide, N-[(1R,2S)-2-hydroxy-1-phenylpropyl]-4-methyl-

There total 2 articles about Benzenesulfonamide, N-[(1R,2S)-2-hydroxy-1-phenylpropyl]-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88082-68-2
(1R,2R)-1-amino-1-phenylpropan-2-ol

: 98-59-9
p-toluenesulfonyl chloride

: 877994-35-9
cis-2-Hydroxy-1-phenyl-1-tosylaminopropan

Guidance literature:: With triethylamine; In tetrahydrofuran; water; at 0 - 20 ℃;
DOI:10.1021/ja802896n

Reference yield:

: 51608-60-7
N-(benzylidene)-p-methylbenzenesulfonamide

: 2,2'-(ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 877994-35-9
cis-2-Hydroxy-1-phenyl-1-tosylaminopropan

: 58107-42-9,58107-44-1
trans-2-Hydroxy-1-phenyl-1-tosylaminopropan

: N-((1S,2R)-2-hydroxy-1-phenylpropyl)-4-methylbenzene sulfonamide

Guidance literature:: 2,2'-(ethane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane); With C₂₄H₂₀NO₃P; copper(I) bromide; lithium tert-butoxide; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere; Glovebox;

N-(benzylidene)-p-methylbenzenesulfonamide; In tetrahydrofuran; at 20 ℃; for 24h; Sealed tube;

With dihydrogen peroxide; sodium hydrogencarbonate; In tetrahydrofuran; water; at 20 ℃; for 3h; Solvent; Reagent/catalyst; Overall yield = 92 %; Overall yield = 56 mg; stereoselective reaction;
DOI:10.1002/anie.201705829