Silane, [[2-[3-(1,1-dimethylethyl)-2-benzostannin-2-yl]-1,3,5-benzenetriyl]trimeth ylidyne]hexakis[trimethyl-

Base Information

Chemical Name:Silane, [[2-[3-(1,1-dimethylethyl)-2-benzostannin-2-yl]-1,3,5-benzenetriyl]trimeth ylidyne]hexakis[trimethyl-
CAS No.:877995-20-5
Molecular Formula:C40H74Si6Sn
Molecular Weight:842.251
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, [[2-[3-(1,1-dimethylethyl)-2-benzostannin-2-yl]-1,3,5-benzenetriyl]trimeth ylidyne]hexakis[trimethyl-

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Silane, [[2-[3-(1,1-dimethylethyl)-2-benzostannin-2-yl]-1,3,5-benzenetriyl]trimeth ylidyne]hexakis[trimethyl-

There total 6 articles about Silane, [[2-[3-(1,1-dimethylethyl)-2-benzostannin-2-yl]-1,3,5-benzenetriyl]trimeth ylidyne]hexakis[trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 877995-22-7
2-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-2-bromo-3-tert-butyl-1,2-dihydro-2-stannanaphthalene

: 877995-20-5
2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-3-tert-butyl-2-stannanaphthalene

Guidance literature:: With lithium diisopropylamide; In hexane; at -40°C to room temp.;
DOI:10.1021/ja057531d

Reference yield: 49.0%

: 877995-22-7
2-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-2-bromo-3-tert-butyl-1,2-dihydro-2-stannanaphthalene

: 1068655-40-2
2-(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)-2-chloro-3-tert-butyl-1,2-dihydro-2-stannanaphthalene

: 877995-20-5
2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-3-tert-butyl-2-stannanaphthalene

Guidance literature:: With lithium 2,2,6,6-tetramethylpiperidide; In tetrahydrofuran; hexane; (Ar); soln. of piperidide in THF was added to mixt. of Sn compd. in hexane at -40°C in glovebox; stirred at room temp. for 0.5 h; solvent removed (vac.); hexane added; filtered through Celite; solvent removed; recrystd. (hexane);
DOI:10.1039/b718193k

Reference yield:

: 211508-96-2
3-tert-butyl-1H-isotellurochromene

: 877995-20-5
2-(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-3-tert-butyl-2-stannanaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: n-BuLi; LiAlH₄ / tetrahydrofuran

2: benzene

3: lithium diisopropylamide / hexane

With n-BuLi; LiAlH₄; lithium diisopropylamide; In tetrahydrofuran; hexane; benzene;
DOI:10.1021/ja057531d