cobalt(2+) 2,7,12,17-tetraethyl-3,8,13,18-tetramethylporphine-21,22-diide

Base Information

Chemical Name:cobalt(2+) 2,7,12,17-tetraethyl-3,8,13,18-tetramethylporphine-21,22-diide
CAS No.:14055-17-5
Molecular Formula:C₃₂H₃₆CoN₄
Molecular Weight:535.658
Hs Code.:
Mol file:14055-17-5.mol

Synonyms:Cobalt,[2,7,12,17-tetraethyl-3,8,13,18-tetramethyl-21H,23H-porphinato(2-)-N21,N22,N23,N24]-,(SP-4-1)-; Cobalt, [2,7,12,17-tetraethyl-3,8,13,18-tetramethylporphinato(2-)]-(8CI); Cobalt, [etioporphyrin 1-ato(2-)]- (7CI); Etioporphyrin I, Co deriv.(6CI); 21H,23H-Porphine, 2,7,12,17-tetraethyl-3,8,13,18-tetramethyl-, cobaltcomplex; Cobalt etioporphyrin I; Cobalt(2+) etioporphyrin; Cobalt(II)etioporphyrin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cobalt(2+) 2,7,12,17-tetraethyl-3,8,13,18-tetramethylporphine-21,22-diide

Chemical Property:

Vapor Pressure:1.79E-24mmHg at 25°C
Boiling Point:797.9°Cat760mmHg
Flash Point:341.3°C
PSA：15.88000
Density:g/cm³
LogP:4.84600

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of cobalt(2+) 2,7,12,17-tetraethyl-3,8,13,18-tetramethylporphine-21,22-diide

There total 1 articles about cobalt(2+) 2,7,12,17-tetraethyl-3,8,13,18-tetramethylporphine-21,22-diide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.5%

: 4949-42-2
4-ethyl-5-formyl-3-methyl-pyrrole-2-carboxylic acid

: 71-48-7,917-69-1,5931-89-5,55881-15-7,68931-68-0,68931-69-1,93029-27-7
cobalt(II) acetate

: 603-35-0
triphenylphosphine

: 14055-17-5
[(2,7,12,17-tetramethyl-3,8,13,18-tetraethylporphyrinato)cobalt(II)]

: [(triphenylphosphine)(2,7,12,17-tetramethyl-3,8,13,18-tetraethylcorrolato)cobalt(III)]

: [(triphenylphosphine)(2,7,12,17-tetramethyl-3,8,13,18-tetraethylcorrolato)cobalt(III)]

: [(triphenylphosphine)(2,7,13,18-tetramethyl-3,8,12,17-tetraethylcorrolato)cobalt(III)]

Guidance literature:: With sodium acetate; trifluoroacetic acid; In ethanol; refluxing substituted pyrrole with CF3CO2H for 30 min, addn. of AcONa, Co-salt and PPh3, refluxing for 24 h; evapn. (vac.), extn. into Et2O, chromy. (Al2O3, Et2O; then Al2O3, Et2O/hexane=1:3), fractional crystn. (pentane, -30°C); elem. anal.;
DOI:10.1016/0020-1693(95)04747-6