2-Naphthalenecarboxamide, 3-hydroxy-N-(4-nitrophenyl)-

Base Information

Chemical Name:2-Naphthalenecarboxamide, 3-hydroxy-N-(4-nitrophenyl)-
CAS No.:2208-20-0
Molecular Formula:C17H12 N2 O4
Molecular Weight:308.293
Hs Code.:2924299090
European Community (EC) Number:606-926-7
NSC Number:37608
UNII:98QD7VL4MX
DSSTox Substance ID:DTXSID6062252
Wikidata:Q81989935
ChEMBL ID:CHEMBL294267
Mol file:2208-20-0.mol

Synonyms:2208-20-0;2-Naphthalenecarboxamide, 3-hydroxy-N-(4-nitrophenyl)-;Naphthol AS-AN;3-hydroxy-N-(4-nitrophenyl)naphthalene-2-carboxamide;3-hydroxy-4'-nitro-2-naphthanilide;98QD7VL4MX;CHEMBL294267;C.I. 37516;C.I. Azoic Coupling Component 27;NSC-37608;Naphthol AS-AN (C.I. 37516);2-Naphthanilide, 3-hydroxy-4'-nitro-;3-hydroxy-N-(4-nitrophenyl)-2-Naphthalenecarboxamide;UNII-98QD7VL4MX;SCHEMBL9120655;DTXSID6062252;NSC37608;BDBM50091998;NSC 37608;FT-0757849;(3-Hydroxy(2-naphthyl))-N-(4-nitrophenyl)carboxamide;3-Hydroxy-naphthalene-2-carboxylic acid (4-nitro-phenyl)-amide

Suppliers and Price of 2-Naphthalenecarboxamide, 3-hydroxy-N-(4-nitrophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 11 raw suppliers

Chemical Property of 2-Naphthalenecarboxamide, 3-hydroxy-N-(4-nitrophenyl)-

Chemical Property:

Vapor Pressure:2.76E-09mmHg at 25°C
Boiling Point:465.5°Cat760mmHg
Flash Point:235.3°C
PSA：95.15000
Density:1.449g/cm³
LogP:4.30210
XLogP3:4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:308.07970687
Heavy Atom Count:23
Complexity:442

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C=C(C(=CC2=C1)C(=O)NC3=CC=C(C=C3)[N+](=O)[O-])O

Technology Process of 2-Naphthalenecarboxamide, 3-hydroxy-N-(4-nitrophenyl)-

There total 3 articles about 2-Naphthalenecarboxamide, 3-hydroxy-N-(4-nitrophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 100-01-6,104810-17-5
4-nitro-aniline

: 92-70-6
3-Hydroxy-2-naphthoic acid

: 2208-20-0
3-hydroxy-N-(4-nitrophenyl)naphthalene-2-carboxamide

Guidance literature:: With phosphorus trichloride; In chlorobenzene; at 100 - 130 ℃; for 0.75h; Microwave irradiation;
DOI:10.3390/molecules18077977

Reference yield:

: 1734-00-5
3-hydroxy-2-naphthoyl chloride

: 100-01-6,104810-17-5
4-nitro-aniline

: 2208-20-0
3-hydroxy-N-(4-nitrophenyl)naphthalene-2-carboxamide

Guidance literature:: With sodium acetate; In N,N-dimethyl-formamide; chlorobenzene; at 5 - 50 ℃;

Reference yield:

: 92-70-6
3-Hydroxy-2-naphthoic acid

: 2208-20-0
3-hydroxy-N-(4-nitrophenyl)naphthalene-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / nitrobenzene

2: 5 h / 130 - 140 °C

With thionyl chloride; In nitrobenzene;