1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid, 6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-3-[[1-(phenylmethyl)-3-azetidinyl] thio]-, (4-nitrophenyl)methyl ester, (4R,5S,6S)-

Base Information

Chemical Name:1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid, 6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-3-[[1-(phenylmethyl)-3-azetidinyl] thio]-, (4-nitrophenyl)methyl ester, (4R,5S,6S)-
CAS No.:878391-75-4
Molecular Formula:C27H29N3O6S
Molecular Weight:523.61
Hs Code.:

1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid,
6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-3-[[1-(phenylmethyl)-3-azetidinyl]
thio]-, (4-nitrophenyl)methyl ester, (4R,5S,6S)-

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Chemical Property of 1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid, 6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-3-[[1-(phenylmethyl)-3-azetidinyl] thio]-, (4-nitrophenyl)methyl ester, (4R,5S,6S)-

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Technology Process of 1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid, 6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-3-[[1-(phenylmethyl)-3-azetidinyl] thio]-, (4-nitrophenyl)methyl ester, (4R,5S,6S)-

There total 1 articles about 1-Azabicyclo[3.2.0]hept-2-ene-2-carboxylic acid, 6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-3-[[1-(phenylmethyl)-3-azetidinyl] thio]-, (4-nitrophenyl)methyl ester, (4R,5S,6S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 878391-63-0
1-benzylazetidine-3-thiol

: 93711-81-0,90776-59-3,189188-38-3
(4-nitrophenyl)methyl (4R,5R,6S)-3-[(diphenoxyphosphinyl)oxy]-6-[(1R)-1-hydroxyethyl]-4-methyl-7-oxo-1-azabicyclo[3.2.0]hept-2-ene-2-carboxylate

: 878391-75-4
4-nitrobenzyl (1R,5S,6S)-2-(1-benzyl-azetidine-3-yl-thio)-6-[(1R)-1-hydroxylethyl]-1-methylcarbapen-2-em-3-ester carboxylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at -20 - -10 ℃; for 2h;

Reference yield: 27.0%

: 878391-75-4
4-nitrobenzyl (1R,5S,6S)-2-(1-benzyl-azetidine-3-yl-thio)-6-[(1R)-1-hydroxylethyl]-1-methylcarbapen-2-em-3-ester carboxylate

: potassium 4-nitrobenzyl (1R,5S,6S)-2-(1-benzyl-azetidine-3-yl-thio)-6-[(1R)-1-hydroxylethyl]-1-methylcarbapen-2-em-3-carboxylate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; water; at 20 ℃; for 3h; pH=7; Potassium phosphate buffer;