Disulfide, bis(2-chloro-2-phenylethyl)

Base Information

• Chemical Name: Disulfide, bis(2-chloro-2-phenylethyl)
• CAS No.: 29184-39-2
• Molecular Formula: C16H16 Cl2 S2
• Molecular Weight: 343.341
• Hs Code.: 2930909090
• European Community (EC) Number: 249-493-6
• DSSTox Substance ID: DTXSID30885448
• Nikkaji Number: J250.790K
• Mol file: 29184-39-2.mol

Synonyms:Disulfide, bis(2-chloro-2-phenylethyl);29184-39-2;Bis(2-chlorophenethyl) disulphide;SCHEMBL11460830;DTXSID30885448;EINECS 249-493-6;Bis(2-chloro-2-phenylethyl) persulfide

Chemical Property of Disulfide, bis(2-chloro-2-phenylethyl)

Chemical Property:

• Vapor Pressure: 1.11E-07mmHg at 25°C
• Boiling Point: 444.6°Cat760mmHg
• Flash Point: 204.7°C
• PSA: 50.60000
• Density: 1.28g/cm³
• LogP: 6.32800
• XLogP3: 5.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 7
• Exact Mass: 342.0070482
• Heavy Atom Count: 20
• Complexity: 225

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(CSSCC(C2=CC=CC=C2)Cl)Cl

Technology Process of Disulfide, bis(2-chloro-2-phenylethyl)

There total 4 articles about Disulfide, bis(2-chloro-2-phenylethyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + dimethylsulfide (75-18-3) → bis(2-phenyl-2-chloroethyl) disulfide (29184-39-2) + Di(2-chloro-2-phenylethyl) sulfide (29713-21-1) + (2-chloro-1-phenyl-ethyl)-dimethyl-sulfonium; chloride

Guidance literature:

With sulfur dichloride; In dichloromethane; at -40 ℃; for 4h;

DOI:10.1023/A:1020933005986

Reference yield:

(2-chloro-2-phenyl-ethylsulfanylmethyl)-dimethyl-amine (802320-19-0) → bis(2-phenyl-2-chloroethyl) disulfide (29184-39-2)

Guidance literature:

With iodine; In diethyl ether;

Reference yield:

2-Dimethylaminomethylsulfanyl-1-phenyl-ethanol; hydrochloride → bis(2-phenyl-2-chloroethyl) disulfide (29184-39-2)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / acetonitrile

2: I₂ / diethyl ether

With thionyl chloride; iodine; In diethyl ether; acetonitrile;

upstream raw materials:

(2-chloro-2-phenyl-ethylsulfanylmethyl)-dimethyl-amine

styrene

dimethylsulfide

Downstream raw materials:

2-Chlor-2-phenyl-ethansulfonylchlorid