Carbamic acid, [(1S)-1-[(1R)-1-hydroxy-2-oxo-2-[[(1R)-1-phenylethyl]amino]ethyl]pentyl]- , (3S)-4,4-dimethyl-1-(phenylmethyl)-3-pyrrolidinyl ester

Base Information

Chemical Name:Carbamic acid, [(1S)-1-[(1R)-1-hydroxy-2-oxo-2-[[(1R)-1-phenylethyl]amino]ethyl]pentyl]- , (3S)-4,4-dimethyl-1-(phenylmethyl)-3-pyrrolidinyl ester
CAS No.:879395-79-6
Molecular Formula:C29H41N3O4
Molecular Weight:495.662
Hs Code.:

Carbamic acid,
[(1S)-1-[(1R)-1-hydroxy-2-oxo-2-[[(1R)-1-phenylethyl]amino]ethyl]pentyl]-
, (3S)-4,4-dimethyl-1-(phenylmethyl)-3-pyrrolidinyl ester

Synonyms:

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Chemical Property of Carbamic acid, [(1S)-1-[(1R)-1-hydroxy-2-oxo-2-[[(1R)-1-phenylethyl]amino]ethyl]pentyl]- , (3S)-4,4-dimethyl-1-(phenylmethyl)-3-pyrrolidinyl ester

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Technology Process of Carbamic acid, [(1S)-1-[(1R)-1-hydroxy-2-oxo-2-[[(1R)-1-phenylethyl]amino]ethyl]pentyl]- , (3S)-4,4-dimethyl-1-(phenylmethyl)-3-pyrrolidinyl ester

There total 5 articles about Carbamic acid, [(1S)-1-[(1R)-1-hydroxy-2-oxo-2-[[(1R)-1-phenylethyl]amino]ethyl]pentyl]- , (3S)-4,4-dimethyl-1-(phenylmethyl)-3-pyrrolidinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 511268-36-3
Methanesulfonic acid (S)-3-hydroxy-4-methanesulfonyloxy-2,2-dimethyl-butyl ester

: 879395-79-6
{(S)-1-[(R)-Hydroxy-((R)-1-phenyl-ethylcarbamoyl)-methyl]-pentyl}-carbamic acid (S)-1-benzyl-4,4-dimethyl-pyrrolidin-3-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / ethanol / 120 °C

2: toluene; pyridine; CH₂Cl₂ / 0 - 20 °C

3: Et₃N / tetrahydrofuran

With triethylamine; In tetrahydrofuran; pyridine; ethanol; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2005.11.101

Reference yield:

: 137161-74-1
(2S)-3,3-dimethylbutane-1,2,4-triol

: 879395-79-6
{(S)-1-[(R)-Hydroxy-((R)-1-phenyl-ethylcarbamoyl)-methyl]-pentyl}-carbamic acid (S)-1-benzyl-4,4-dimethyl-pyrrolidin-3-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 52 percent / pyridine / 0 - 20 °C

2: 90 percent / ethanol / 120 °C

3: toluene; pyridine; CH₂Cl₂ / 0 - 20 °C

4: Et₃N / tetrahydrofuran

With triethylamine; In tetrahydrofuran; pyridine; ethanol; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2005.11.101

Reference yield:

: 144043-26-5
(3S)-N-benzyl-4,4-dimethyl-3-hydroxypyrrolidine

: 879395-79-6
{(S)-1-[(R)-Hydroxy-((R)-1-phenyl-ethylcarbamoyl)-methyl]-pentyl}-carbamic acid (S)-1-benzyl-4,4-dimethyl-pyrrolidin-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene; pyridine; CH₂Cl₂ / 0 - 20 °C

2: Et₃N / tetrahydrofuran

With triethylamine; In tetrahydrofuran; pyridine; dichloromethane; toluene;
DOI:10.1016/j.bmcl.2005.11.101