Propanoic acid, 2-methyl-2-[2-methyl-4-[[2-[[4-(trifluoromethyl)phenoxy]methyl]-2-propen yl]thio]phenoxy]-, ethyl ester

Base Information

• Chemical Name: Propanoic acid, 2-methyl-2-[2-methyl-4-[[2-[[4-(trifluoromethyl)phenoxy]methyl]-2-propen yl]thio]phenoxy]-, ethyl ester
• CAS No.: 879492-48-5
• Molecular Formula: C24H27F3O4S
• Molecular Weight: 468.537
• Mol file: 879492-48-5.mol

Synonyms:

Chemical Property of Propanoic acid, 2-methyl-2-[2-methyl-4-[[2-[[4-(trifluoromethyl)phenoxy]methyl]-2-propen yl]thio]phenoxy]-, ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Propanoic acid, 2-methyl-2-[2-methyl-4-[[2-[[4-(trifluoromethyl)phenoxy]methyl]-2-propen yl]thio]phenoxy]-, ethyl ester

There total 1 articles about Propanoic acid, 2-methyl-2-[2-methyl-4-[[2-[[4-(trifluoromethyl)phenoxy]methyl]-2-propen yl]thio]phenoxy]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

2-(4-mercapto-2-methyl-phenoxy)-2-methyl-propionic acid ethyl ester (447406-77-1) + 2-(4-Trifluoromethyl-phenoxymethyl)-prop-2-en-1-ol (849442-18-8) → 2-Methyl-2-{2-methyl-4-[2-(4-trifluoromethyl-phenoxymethyl)-allylsulfanyl]-phenoxy}-propionic Acid Ethyl Ester (879492-48-5)

Guidance literature:

2-(4-Trifluoromethyl-phenoxymethyl)-prop-2-en-1-ol; With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 2.16667h;

2-(4-mercapto-2-methyl-phenoxy)-2-methyl-propionic acid ethyl ester; With caesium carbonate; In acetonitrile; at 20 ℃; for 3h;

Reference yield: 47.0%

2-Methyl-2-{2-methyl-4-[2-(4-trifluoromethyl-phenoxymethyl)-allylsulfanyl]-phenoxy}-propionic Acid Ethyl Ester (879492-48-5) → 2-methyl-2-{2-methyl-4-[2-(4-trifluoromethyl-phenoxymethyl)-allylsulfanyl]-phenoxy}-propionic acid (879492-46-3)

Guidance literature:

2-Methyl-2-{2-methyl-4-[2-(4-trifluoromethyl-phenoxymethyl)-allylsulfanyl]-phenoxy}-propionic Acid Ethyl Ester; With sodium hydroxide; water; In tetrahydrofuran; methanol; at 25 ℃; for 4h;

With hydrogenchloride; In tetrahydrofuran; methanol; diethyl ether; water;

upstream raw materials:

2-(4-mercapto-2-methyl-phenoxy)-2-methyl-propionic acid ethyl ester

2-(4-Trifluoromethyl-phenoxymethyl)-prop-2-en-1-ol

Downstream raw materials:

2-methyl-2-{2-methyl-4-[2-(4-trifluoromethyl-phenoxymethyl)-allylsulfanyl]-phenoxy}-propionic acid

Refernces