Technology Process of 6-O-decanoyl-3,4-di-O-isobutyrylsucrose
There total 7 articles about 6-O-decanoyl-3,4-di-O-isobutyrylsucrose which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethanol;
for 16h;
under 3000.2 Torr;
DOI:10.1016/0008-6215(90)80128-P
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 94 percent / sodium hydride / dimethylformamide / 2 h
2: 203 mg / 90percent aq. acetic acid / acetonitrile / 3 h
3: 91 percent / pyridine / 6 h
4: tris(triphenylphosphine)rhodium(I) chloride / ethanol; toluene; H2O / 3 h / Heating
5: 116 mg / mercury(II) bromide / ethanol; toluene; H2O / 3 h / Ambient temperature
6: 95 percent / pyridine / 2 h / Ambient temperature
7: 72 percent / H2 / 10percent Pd-C / ethanol / 16 h / 3000.2 Torr
With
pyridine; Wilkinson's catalyst; hydrogen; sodium hydride; acetic acid; mercury dibromide;
palladium on activated charcoal;
In
ethanol; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1016/0008-6215(90)80128-P
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / pyridine / 6 h
2: tris(triphenylphosphine)rhodium(I) chloride / ethanol; toluene; H2O / 3 h / Heating
3: 116 mg / mercury(II) bromide / ethanol; toluene; H2O / 3 h / Ambient temperature
4: 95 percent / pyridine / 2 h / Ambient temperature
5: 72 percent / H2 / 10percent Pd-C / ethanol / 16 h / 3000.2 Torr
With
pyridine; Wilkinson's catalyst; hydrogen; mercury dibromide;
palladium on activated charcoal;
In
ethanol; water; toluene;
DOI:10.1016/0008-6215(90)80128-P
