Methanone, (2-amino-4,5,6,7-tetrahydrobenzo[b]thien-3-yl)(4-chloro-3,5-diiodophen yl)-

Base Information

Chemical Name:Methanone, (2-amino-4,5,6,7-tetrahydrobenzo[b]thien-3-yl)(4-chloro-3,5-diiodophen yl)-
CAS No.:880359-28-4
Molecular Formula:C15H12ClI2NOS
Molecular Weight:543.594
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanone, (2-amino-4,5,6,7-tetrahydrobenzo[b]thien-3-yl)(4-chloro-3,5-diiodophen yl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanone, (2-amino-4,5,6,7-tetrahydrobenzo[b]thien-3-yl)(4-chloro-3,5-diiodophen yl)-

There total 2 articles about Methanone, (2-amino-4,5,6,7-tetrahydrobenzo[b]thien-3-yl)(4-chloro-3,5-diiodophen yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 860697-28-5
4-chloro-3,5-diiodobenzoic methyl ester

: 880359-28-4
(2-amino-4,5,6,7-tetrahydro-benzo[b]thiophen-3-yl)-(4-chloro-3,5-diiodo-phenyl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: NaH

2: S; morpholine / ethanol

With morpholine; sodium hydride; sulfur; In ethanol;
DOI:10.1016/j.bmcl.2005.11.037

Reference yield:

: 880359-27-3
3-(4-chloro-3,5-diiodo-phenyl)-3-oxo-propionitrile

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 880359-28-4
(2-amino-4,5,6,7-tetrahydro-benzo[b]thiophen-3-yl)-(4-chloro-3,5-diiodo-phenyl)-methanone

Guidance literature:: With morpholine; sulfur; In ethanol;
DOI:10.1016/j.bmcl.2005.11.037

Reference yield: 80.0%

: 880359-28-4
(2-amino-4,5,6,7-tetrahydro-benzo[b]thiophen-3-yl)-(4-chloro-3,5-diiodo-phenyl)-methanone

: 40312-34-3
(2-Amino-4,5,6,7-tetrahydrobenzo[b]thiophen-3-yl)(4-chlorophenyl)methanone

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; under 2585.74 Torr;
DOI:10.1016/j.bmcl.2005.11.037