Glycine, L-g-glutamyl-S-[10-carboxy-4-hydroxy-1-(1-hydroxy-3-nonenyl)-2,6-decadienyl]-L-cysteinyl-(9CI)

Base Information

Chemical Name:Glycine, L-g-glutamyl-S-[10-carboxy-4-hydroxy-1-(1-hydroxy-3-nonenyl)-2,6-decadienyl]-L-cysteinyl-(9CI)
CAS No.:130606-48-3
Molecular Formula:C₃₀H₄₉N₃O₁₀S
Molecular Weight:643.799
Hs Code.:

Synonyms:Glycine,N-[S-[10-carboxy-4-hydroxy-1-(1-hydroxy-3-nonenyl)-2,6-decadienyl]-N-L-g-glutamyl-L-cysteinyl]-;Hepoxilin A3-C

Suppliers and Price of Glycine, L-g-glutamyl-S-[10-carboxy-4-hydroxy-1-(1-hydroxy-3-nonenyl)-2,6-decadienyl]-L-cysteinyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of Glycine, L-g-glutamyl-S-[10-carboxy-4-hydroxy-1-(1-hydroxy-3-nonenyl)-2,6-decadienyl]-L-cysteinyl-(9CI)

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Glycine, L-g-glutamyl-S-[10-carboxy-4-hydroxy-1-(1-hydroxy-3-nonenyl)-2,6-decadienyl]-L-cysteinyl-(9CI)

There total 6 articles about Glycine, L-g-glutamyl-S-[10-carboxy-4-hydroxy-1-(1-hydroxy-3-nonenyl)-2,6-decadienyl]-L-cysteinyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (5Z,9E,14Z)-(8R,11R,12S)-8,12-Dihydroxy-11-{(R)-2-(methoxycarbonylmethyl-carbamoyl)-2-[(R)-4-methoxycarbonyl-4-(2,2,2-trifluoro-acetylamino)-butyrylamino]-ethylsulfanyl}-icosa-5,9,14-trienoic acid methyl ester

: 127060-76-8,127128-05-6,127708-68-3,127758-67-2,130606-48-3
(5Z,9E,14Z)-(8R,11R,12S)-11-[(R)-2-((R)-4-Amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethylsulfanyl]-8,12-dihydroxy-icosa-5,9,14-trienoic acid

Guidance literature:: With potassium carbonate; In methanol; water; at 23 ℃; for 24h;
DOI:10.1016/0040-4039(90)80085-Z

Reference yield:

: (5Z,9E,14Z)-(8S,11R,12S)-8,12-Dihydroxy-11-{(R)-2-(methoxycarbonylmethyl-carbamoyl)-2-[(R)-4-methoxycarbonyl-4-(2,2,2-trifluoro-acetylamino)-butyrylamino]-ethylsulfanyl}-icosa-5,9,14-trienoic acid methyl ester

: 127060-76-8,127128-05-6,127708-68-3,127758-67-2,130606-48-3
(5Z,9E,14Z)-(8S,11R,12S)-11-[(R)-2-((R)-4-Amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethylsulfanyl]-8,12-dihydroxy-icosa-5,9,14-trienoic acid

Guidance literature:: With potassium carbonate; In methanol; water; at 23 ℃; for 24h;
DOI:10.1016/0040-4039(90)80085-Z

Reference yield:

: 75290-61-8
N-Trifluoroacetylglutathione dimethyl ester

: 127060-76-8,127128-05-6,127708-68-3,127758-67-2,130606-48-3
(5Z,9E,14Z)-(8R,11R,12S)-11-[(R)-2-((R)-4-Amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethylsulfanyl]-8,12-dihydroxy-icosa-5,9,14-trienoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol / 24 h / 80 °C

2: 0.15 M potasium carbonate / methanol; H₂O / 24 h / 23 °C

With potassium carbonate; triethylamine; In methanol; water;
DOI:10.1016/0040-4039(90)80085-Z