(1S,15S)-21,22,26-trimethoxy-16,31-dimethyl-8,24-dioxa-16,31-diazaheptacyclo[23.6.2.1~3,7~.1~9,13~.1~15,19~.0~23,34~.0~28,32~]hexatriaconta-3(36),4,6,9(35),10,12,19(34),20,22,25,27,32-dodecaen-10-ol (non-preferred name)

Base Information

Chemical Name:(1S,15S)-21,22,26-trimethoxy-16,31-dimethyl-8,24-dioxa-16,31-diazaheptacyclo[23.6.2.1~3,7~.1~9,13~.1~15,19~.0~23,34~.0~28,32~]hexatriaconta-3(36),4,6,9(35),10,12,19(34),20,22,25,27,32-dodecaen-10-ol (non-preferred name)
CAS No.:26137-45-1
Molecular Formula:C37H40 N2 O6
Molecular Weight:608.734
Hs Code.:

(1S,15S)-21,22,26-trimethoxy-16,31-dimethyl-8,24-dioxa-16,31-diazaheptacyclo[23.6.2.1~3,7~.1~9,13~.1~15,19~.0~23,34~.0~28,32~]hexatriaconta-3(36),4,6,9(35),10,12,19(34),20,22,25,27,32-dodecaen-10-ol (non-preferred name)

Synonyms:Berbaman-12-ol,6,6',7-trimethoxy-2,2'-dimethyl-, (1b)-; Penduline (Cocculus) (8CI); (+)-Penduline;16H-1,24:6,9-Dietheno-11,15-metheno-2H-pyrido[2',3':17,18][1,11]dioxacycloeicosino[2,3,4-ij]isoquinolin-12-ol,3,4,4a,5,16a,17,18,19-octahydro-21,22,26-trimethoxy-4,17-dimethyl-,[4aS-(4aR*,16aR*)]-; Penduline

Suppliers and Price of (1S,15S)-21,22,26-trimethoxy-16,31-dimethyl-8,24-dioxa-16,31-diazaheptacyclo[23.6.2.1~3,7~.1~9,13~.1~15,19~.0~23,34~.0~28,32~]hexatriaconta-3(36),4,6,9(35),10,12,19(34),20,22,25,27,32-dodecaen-10-ol (non-preferred name)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,15S)-21,22,26-trimethoxy-16,31-dimethyl-8,24-dioxa-16,31-diazaheptacyclo[23.6.2.1~3,7~.1~9,13~.1~15,19~.0~23,34~.0~28,32~]hexatriaconta-3(36),4,6,9(35),10,12,19(34),20,22,25,27,32-dodecaen-10-ol (non-preferred name)

Chemical Property:

Vapor Pressure:4.62E-21mmHg at 25°C
Boiling Point:714°Cat760mmHg
Flash Point:385.6°C
Density:1.204g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (1S,15S)-21,22,26-trimethoxy-16,31-dimethyl-8,24-dioxa-16,31-diazaheptacyclo[23.6.2.1~3,7~.1~9,13~.1~15,19~.0~23,34~.0~28,32~]hexatriaconta-3(36),4,6,9(35),10,12,19(34),20,22,25,27,32-dodecaen-10-ol (non-preferred name)

There total 4 articles about (1S,15S)-21,22,26-trimethoxy-16,31-dimethyl-8,24-dioxa-16,31-diazaheptacyclo[23.6.2.1~3,7~.1~9,13~.1~15,19~.0~23,34~.0~28,32~]hexatriaconta-3(36),4,6,9(35),10,12,19(34),20,22,25,27,32-dodecaen-10-ol (non-preferred name) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 518-34-3,5990-67-0
Tetrandrin

: 21008-67-3
Atherospermoline

: 26137-45-1
(+)-penduline

: 83087-72-3
6',7-Bis-(O-demethyl)-tetrandrine

: 436-77-1,10172-02-8,33889-68-8,38769-07-2,53834-87-0,119478-08-9
fangchinoline

Guidance literature:: With hydrogen bromide; at 20 ℃; for 24h; Yield given. Further byproducts given;
DOI:10.1002/ardp.19823150705

Reference yield: 35.0%

: 518-34-3,5990-67-0
Tetrandrin

: 83113-25-1
Tetrakis-(O-demethyl)-tetrandrin

: 21008-67-3
Atherospermoline

: 26137-45-1
(+)-penduline

: 83113-24-0
6',7,12-Tris-(O-demethyl)-tetrandrine

: 83087-72-3
6',7-Bis-(O-demethyl)-tetrandrine

: 436-77-1,10172-02-8,33889-68-8,38769-07-2,53834-87-0,119478-08-9
fangchinoline

Guidance literature:: With hydrogen bromide; at 20 ℃; for 24h; Product distribution; different concentration of HBr, different times and temperatures;
DOI:10.1002/ardp.19823150705

Reference yield: 25.0%

: 478-61-5,569-16-4,26137-45-1,64665-35-6
berbamine

: 26137-45-1
(+)-penduline

Guidance literature:: With methanol; oxygen; at 40 ℃; for 24h; Product distribution; Mechanism; other bisbenzylisoquinoline alkaloids;
DOI:10.3987/COM-95-7155