Carbamic acid, [(1S)-2-[[2-[(1Z)-3-(acetyloxy)-1-propenyl]phenyl]amino]-1-[[[(1,1-dimeth ylethyl)dimethylsilyl]oxy]methyl]-2-oxoethyl]-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S)-2-[[2-[(1Z)-3-(acetyloxy)-1-propenyl]phenyl]amino]-1-[[[(1,1-dimeth ylethyl)dimethylsilyl]oxy]methyl]-2-oxoethyl]-, phenylmethyl ester
CAS No.:881027-40-3
Molecular Formula:C₂₈H₃₈N₂O₆Si
Molecular Weight:526.705
Hs Code.:

Carbamic acid,
[(1S)-2-[[2-[(1Z)-3-(acetyloxy)-1-propenyl]phenyl]amino]-1-[[[(1,1-dimeth
ylethyl)dimethylsilyl]oxy]methyl]-2-oxoethyl]-, phenylmethyl ester

Synonyms:

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Chemical Property of Carbamic acid, [(1S)-2-[[2-[(1Z)-3-(acetyloxy)-1-propenyl]phenyl]amino]-1-[[[(1,1-dimeth ylethyl)dimethylsilyl]oxy]methyl]-2-oxoethyl]-, phenylmethyl ester

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Technology Process of Carbamic acid, [(1S)-2-[[2-[(1Z)-3-(acetyloxy)-1-propenyl]phenyl]amino]-1-[[[(1,1-dimeth ylethyl)dimethylsilyl]oxy]methyl]-2-oxoethyl]-, phenylmethyl ester

There total 1 articles about Carbamic acid, [(1S)-2-[[2-[(1Z)-3-(acetyloxy)-1-propenyl]phenyl]amino]-1-[[[(1,1-dimeth ylethyl)dimethylsilyl]oxy]methyl]-2-oxoethyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: {(S)-2-(tert-Butyl-dimethyl-silanyloxy)-1-[2-((Z)-3-hydroxy-propenyl)-phenylcarbamoyl]-ethyl}-carbamic acid benzyl ester

: 108-24-7
acetic anhydride

: 881027-40-3
Acetic acid (Z)-3-{2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-propionylamino]-phenyl}-allyl ester

Guidance literature:: With pyridine; at 20 ℃;
DOI:10.3987/COM-05-S(K)11

Reference yield:

: 881027-40-3
Acetic acid (Z)-3-{2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-propionylamino]-phenyl}-allyl ester

: 881027-48-1
acetic acid 2-{2-[1-benzyloxycarbonylamino-2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-1H-indol-3-yl}-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Lawesson's reagent; pyridine / toluene / 0.17 h / Heating

2: 84 percent / (n-Bu)3SnH; Et₃B / tetrahydrofuran; toluene / 0.5 h / 20 °C

With Lawessons reagent; pyridine; triethyl borane; tri-n-butyl-tin hydride; In tetrahydrofuran; toluene;
DOI:10.3987/COM-05-S(K)11

Reference yield:

: 881027-40-3
Acetic acid (Z)-3-{2-[(S)-2-benzyloxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-propionylamino]-phenyl}-allyl ester

: 881027-58-3
2-[1-benzyloxycarbonylamino-2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-3-(2-hydroxy-ethyl)-indole-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Lawesson's reagent; pyridine / toluene / 0.17 h / Heating

2: 84 percent / (n-Bu)3SnH; Et₃B / tetrahydrofuran; toluene / 0.5 h / 20 °C

3: 81 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

4: 75 percent / K₂CO₃ / methanol / 20 °C

With Lawessons reagent; pyridine; dmap; triethyl borane; tri-n-butyl-tin hydride; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.3987/COM-05-S(K)11