(+-)-2-alpha,6-beta-Diethyl-3-beta-(p-hydroxyphenyl)-trans-bicyclo(4.3.0)nonan-7-beta-ol

Base Information

Chemical Name:(+-)-2-alpha,6-beta-Diethyl-3-beta-(p-hydroxyphenyl)-trans-bicyclo(4.3.0)nonan-7-beta-ol
CAS No.:71782-95-1
Molecular Formula:C₁₉H₂₈O₂
Molecular Weight:288.43
Hs Code.:
DSSTox Substance ID:DTXSID80992434
Wikidata:Q82982595

Synonyms:(+-)-2-alpha,6-beta-Diethyl-3-beta-(p-hydroxyphenyl)-trans-bicyclo(4.3.0)nonan-7-beta-ol;1H-Inden-1-ol, octahydro-4,7a-diethyl-5-(4-hydroxyphenyl)-, (1-alpha,3a-beta,4-beta,5-alpha,7a-alpha)-(+-)-;71782-95-1;DTXSID80992434;LS-81800;4,7a-Diethyl-5-(4-hydroxyphenyl)octahydro-1H-inden-1-ol

Suppliers and Price of (+-)-2-alpha,6-beta-Diethyl-3-beta-(p-hydroxyphenyl)-trans-bicyclo(4.3.0)nonan-7-beta-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (+-)-2-alpha,6-beta-Diethyl-3-beta-(p-hydroxyphenyl)-trans-bicyclo(4.3.0)nonan-7-beta-ol

Chemical Property:

Vapor Pressure:3.3E-08mmHg at 25°C
Boiling Point:431.4°C at 760 mmHg
Flash Point:195.7°C
Density:1.067g/cm³
XLogP3:4.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:288.208930132
Heavy Atom Count:21
Complexity:348

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1C(CCC2(C1CCC2O)CC)C3=CC=C(C=C3)O
Isomeric SMILES:CC[C@H]1[C@@H](CC[C@@]2([C@@H]1CC[C@H]2O)CC)C3=CC=C(C=C3)O

Technology Process of (+-)-2-alpha,6-beta-Diethyl-3-beta-(p-hydroxyphenyl)-trans-bicyclo(4.3.0)nonan-7-beta-ol

There total 9 articles about (+-)-2-alpha,6-beta-Diethyl-3-beta-(p-hydroxyphenyl)-trans-bicyclo(4.3.0)nonan-7-beta-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 77814-35-8,95733-44-1,95733-45-2
2α,6β-Diethyl-3β-(p-methoxyphenyl)-trans-bicyclo<4.3.0>nonan-7β-ol

: 71782-95-1,95733-46-3,95733-49-6
(+/-) 2α,6β-diethyl-3β-(p-hydroxyphenyl)-trans-bicyclo<4.3.0>nonan-7β-ol

Guidance literature:: With potassium hydroxide; In diethylene glycol; at 220 - 230 ℃; for 1.5h;

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 71782-95-1,95733-46-3,95733-49-6
(+/-) 2α,6β-diethyl-3β-(p-hydroxyphenyl)-trans-bicyclo<4.3.0>nonan-7β-ol

Guidance literature:: Multi-step reaction with 4 steps

2: 97 percent / H₂ / 10percent Pd/C / ethanol

3: 78 percent / K/liquid NH₃ / dioxane; diethyl ether / 2 h / -50 °C

4: 60 percent / KOH / bis-(2-hydroxy-ethyl) ether / 1.5 h / 220 - 230 °C

With potassium hydroxide; ammonia; hydrogen; palladium on activated charcoal; In 1,4-dioxane; diethyl ether; ethanol; diethylene glycol;

Reference yield:

: 1629-60-3
1-hexene-3-one

: 71782-95-1,95733-46-3,95733-49-6
(+/-) 2α,6β-diethyl-3β-(p-hydroxyphenyl)-trans-bicyclo<4.3.0>nonan-7β-ol

Guidance literature:: Multi-step reaction with 7 steps

1: 77 percent / KOH / methanol / 6 h / Heating

2: 86 percent / TsOH / benzene / 6 h / Heating

3: 89 percent / NaBH₄ / propan-2-ol; ethanol / 1) 0.5, 0 deg C, 2) 1 h, rt

5: 97 percent / H₂ / 10percent Pd/C / ethanol

6: 78 percent / K/liquid NH₃ / dioxane; diethyl ether / 2 h / -50 °C

7: 60 percent / KOH / bis-(2-hydroxy-ethyl) ether / 1.5 h / 220 - 230 °C

With potassium hydroxide; sodium tetrahydroborate; ammonia; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In 1,4-dioxane; methanol; diethyl ether; ethanol; isopropyl alcohol; diethylene glycol; benzene;