Carbamic acid, [(2R,3S)-4-(3,5-difluorophenyl)-3-[[3-[(dipropylamino)carbonyl]-5-methyl benzoyl]amino]-2-hydroxybutyl]methyl-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Carbamic acid, [(2R,3S)-4-(3,5-difluorophenyl)-3-[[3-[(dipropylamino)carbonyl]-5-methyl benzoyl]amino]-2-hydroxybutyl]methyl-, 1,1-dimethylethyl ester
• CAS No.: 881424-44-8
• Molecular Formula: C31H43F2N3O5
• Molecular Weight: 575.696

Synonyms:

Chemical Property of Carbamic acid, [(2R,3S)-4-(3,5-difluorophenyl)-3-[[3-[(dipropylamino)carbonyl]-5-methyl benzoyl]amino]-2-hydroxybutyl]methyl-, 1,1-dimethylethyl ester

Chemical Property:

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Technology Process of Carbamic acid, [(2R,3S)-4-(3,5-difluorophenyl)-3-[[3-[(dipropylamino)carbonyl]-5-methyl benzoyl]amino]-2-hydroxybutyl]methyl-, 1,1-dimethylethyl ester

There total 1 articles about Carbamic acid, [(2R,3S)-4-(3,5-difluorophenyl)-3-[[3-[(dipropylamino)carbonyl]-5-methyl benzoyl]amino]-2-hydroxybutyl]methyl-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methyl-5-[(dipropylamino)carbonyl]benzoic acid (388072-25-1) + (2R,3S)-[3-amino-4-(3,5-difluoro-phenyl)-2-hydroxy-butyl]-methyl-carbamic acid tert-butyl ester (881424-43-7) → (2R,3S)-[4-(3,5-difluoro-phenyl)-3-(3-dipropylcarbamoyl-5-methyl-benzoylamino)-2-hydroxy-butyl]-methyl-carbamic acid tert-butyl ester (881424-44-8)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;

Reference yield:

(2R,3S)-[4-(3,5-difluoro-phenyl)-3-(3-dipropylcarbamoyl-5-methyl-benzoylamino)-2-hydroxy-butyl]-methyl-carbamic acid tert-butyl ester (881424-44-8) → (1S,2R)-N-[1-(3,5-difluoro-benzyl)-2-hydroxy-3-methylamino-propyl]-5-methyl-N',N'-dipropyl-isophthalamide hydrochloride

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1.5h;

upstream raw materials:

3-methyl-5-[(dipropylamino)carbonyl]benzoic acid

(2R,3S)-[3-amino-4-(3,5-difluoro-phenyl)-2-hydroxy-butyl]-methyl-carbamic acid tert-butyl ester

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