Benzenamine, 4,4'-9H-carbazole-3,6-diylbis[N,N-diphenyl-

Base Information

• Chemical Name: Benzenamine, 4,4'-9H-carbazole-3,6-diylbis[N,N-diphenyl-
• CAS No.: 885665-26-9
• Molecular Formula: C48H35N3
• Molecular Weight: 653.826
• Mol file: 885665-26-9.mol

Synonyms:Benzenamine,4,4'-9H-carbazole-3,6-diylbis[N,N-diphenyl;3,6-bis(4-diphenylamino-phenyl)-9H-carbazole;4,4'-(9H-carbazol-3,6-diyl)bis(N,N-diphenylaniline);

Chemical Property of Benzenamine, 4,4'-9H-carbazole-3,6-diylbis[N,N-diphenyl-

Chemical Property:

• PSA: 22.27000
• LogP: 13.59470

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, 4,4'-9H-carbazole-3,6-diylbis[N,N-diphenyl-

There total 5 articles about Benzenamine, 4,4'-9H-carbazole-3,6-diylbis[N,N-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,6-dibromo-9H-carbazole (6825-20-3) + 4-(diphenylamino)phenyl boronic acid (201802-67-7) → 4,4’-(9H-carbazole-3,6-diyl)bis(N,N-diphenylaniline) (885665-26-9)

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; Inert atmosphere; Reflux;

Reference yield: 88.0%

4-(diphenylamino)phenylboronic pinacol ester (267221-88-5) + 3,6-dibromo-9H-carbazole (6825-20-3) → 4,4’-(9H-carbazole-3,6-diyl)bis(N,N-diphenylaniline) (885665-26-9)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; for 48h; Inert atmosphere; Reflux;

Reference yield:

3,6-diiodocarbazole (57103-02-3) + 4-(diphenylamino)phenyl boronic acid (201802-67-7) → 4,4’-(9H-carbazole-3,6-diyl)bis(N,N-diphenylaniline) (885665-26-9)

Guidance literature:

With potassium phosphate; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide; at 45 ℃; for 24h;

upstream raw materials:

3,6-dibromo-9H-carbazole

4-(diphenylamino)phenyl boronic acid

3,6-diiodocarbazole

4-(diphenylamino)phenylboronic pinacol ester

Downstream raw materials:

4,4'-{9-[4-(10-phenyl-9-anthryl)phenyl]-9H-carbazol-3,6-diyl}bis(N,N-diphenylaniline)