Oxirane, [[[3,4-bis(phenylmethoxy)-1-naphthalenyl]oxy]methyl]-

Base Information

Chemical Name:Oxirane, [[[3,4-bis(phenylmethoxy)-1-naphthalenyl]oxy]methyl]-
CAS No.:89710-78-1
Molecular Formula:C₂₇H₂₄O₄
Molecular Weight:412.485
Hs Code.:

Synonyms:

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Chemical Property of Oxirane, [[[3,4-bis(phenylmethoxy)-1-naphthalenyl]oxy]methyl]-

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Technology Process of Oxirane, [[[3,4-bis(phenylmethoxy)-1-naphthalenyl]oxy]methyl]-

There total 6 articles about Oxirane, [[[3,4-bis(phenylmethoxy)-1-naphthalenyl]oxy]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89710-77-0
Toluene-4-sulfonic acid 3-(3,4-bis-benzyloxy-naphthalen-1-yloxy)-2-hydroxy-propyl ester

: 89710-78-1
1-<3,4-bis(benzyloxy)-1-naphthoxy>-2,3-epoxypropane

Guidance literature:: With potassium hydroxide; In pyridine; methanol; for 0.333333h; Yield given;
DOI:10.1021/jm00373a008

Reference yield:

: 42164-68-1
4-(allyloxy)-1,2-naphthoquinone

: 89710-78-1
1-<3,4-bis(benzyloxy)-1-naphthoxy>-2,3-epoxypropane

Guidance literature:: Multi-step reaction with 5 steps

1: sodium dithionite / H₂O

2: K₂CO₃ / dimethylformamide / 24 h / 50 °C

3: 71 percent / N-methylmorpholine N-oxide, osmium tetraoxide stabilized tert-butyl peroxide, water / 2-methyl-propan-2-ol; tetrahydrofuran / 24 h

4: pyridine / 48 h / Ambient temperature

5: KOH / pyridine; methanol / 0.33 h

With pyridine; potassium hydroxide; sodium dithionite; osmium tetraoxide stabilized tert-butyl peroxide; water; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; pyridine; methanol; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm00373a008

Reference yield:

: 36417-25-1
2-hydroxy-1,4-naphthoquinone silver salt

: 89710-78-1
1-<3,4-bis(benzyloxy)-1-naphthoxy>-2,3-epoxypropane

Guidance literature:: Multi-step reaction with 6 steps

1: 40 percent / benzene / 0.33 h / Heating

2: sodium dithionite / H₂O

3: K₂CO₃ / dimethylformamide / 24 h / 50 °C

4: 71 percent / N-methylmorpholine N-oxide, osmium tetraoxide stabilized tert-butyl peroxide, water / 2-methyl-propan-2-ol; tetrahydrofuran / 24 h

5: pyridine / 48 h / Ambient temperature

6: KOH / pyridine; methanol / 0.33 h

With pyridine; potassium hydroxide; sodium dithionite; osmium tetraoxide stabilized tert-butyl peroxide; water; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; pyridine; methanol; water; N,N-dimethyl-formamide; tert-butyl alcohol; benzene;
DOI:10.1021/jm00373a008