Benzenesulfonamide, 4-methyl-N-(8,9,10,11-tetrahydro-9-hydroxybenz[a]anthracen-8-yl)-, trans-

Base Information

Chemical Name:Benzenesulfonamide, 4-methyl-N-(8,9,10,11-tetrahydro-9-hydroxybenz[a]anthracen-8-yl)-, trans-
CAS No.:89817-10-7
Molecular Formula:C₂₅H₂₃NO₃S
Molecular Weight:417.529
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonamide, 4-methyl-N-(8,9,10,11-tetrahydro-9-hydroxybenz[a]anthracen-8-yl)-, trans-

Chemical Property:

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Technology Process of Benzenesulfonamide, 4-methyl-N-(8,9,10,11-tetrahydro-9-hydroxybenz[a]anthracen-8-yl)-, trans-

There total 3 articles about Benzenesulfonamide, 4-methyl-N-(8,9,10,11-tetrahydro-9-hydroxybenz[a]anthracen-8-yl)-, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34501-53-6,77550-46-0
1a,2,3,11b-tetrahydrobenz<5,6>anthra<1,2-b>oxirene

: 89817-10-7
trans-8,9,10,11-tetrahydro-8-(4-methyl)benzenesulfonamidobenz anthr-9-ol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide, / sulfuric acid / H₂O; acetone / 36 h / Ambient temperature

2: 21 percent / trimethyl phosphite / CH₂Cl₂ / 10 h / Heating

3: 1. THF, 40 degC, 2min., then 25 degC, 30min.; 2. 40 degC, 90min.; 3. warm 5percent ammonia, 5percent sodium bicarbonate

With sodium azide; phosphorous acid trimethyl ester; sulfuric acid; In dichloromethane; water; acetone;

Reference yield:

: trans-8-azido-8,9,10,11-tetrahydrobenz anthr-9-ol

: 89817-10-7
trans-8,9,10,11-tetrahydro-8-(4-methyl)benzenesulfonamidobenz anthr-9-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 21 percent / trimethyl phosphite / CH₂Cl₂ / 10 h / Heating

2: 1. THF, 40 degC, 2min., then 25 degC, 30min.; 2. 40 degC, 90min.; 3. warm 5percent ammonia, 5percent sodium bicarbonate

With phosphorous acid trimethyl ester; In dichloromethane;

Reference yield:

: 10416-59-8,132255-83-5
N,O-Bis(trimethylsilyl)acetamide

: 89817-06-1
1a,2,3,11b-tetrahydrobenz<5,6>anthra<1,2-b>azirine

: 98-59-9
p-toluenesulfonyl chloride

: 89817-10-7
trans-8,9,10,11-tetrahydro-8-(4-methyl)benzenesulfonamidobenz anthr-9-ol

Guidance literature:: Yield given. Multistep reaction; 1. THF, 40 degC, 2min., then 25 degC, 30min.; 2. 40 degC, 90min.; 3. warm 5percent ammonia, 5percent sodium bicarbonate;