Piperidine, 3-(3-methoxyphenyl)-1-(phenylmethyl)-, (R)-

Base Information

Chemical Name:Piperidine, 3-(3-methoxyphenyl)-1-(phenylmethyl)-, (R)-
CAS No.:89920-95-6
Molecular Formula:C19H23NO
Molecular Weight:281.398
Hs Code.:

Synonyms:

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Chemical Property of Piperidine, 3-(3-methoxyphenyl)-1-(phenylmethyl)-, (R)-

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Technology Process of Piperidine, 3-(3-methoxyphenyl)-1-(phenylmethyl)-, (R)-

There total 5 articles about Piperidine, 3-(3-methoxyphenyl)-1-(phenylmethyl)-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 88784-36-5
N-benzyl-3-(3-methoxyphenyl)piperidine

: 89920-95-6
N-benzyl-3(R)-(3-methoxyphenyl)piperidine

Guidance literature:: With O,O'-dibenzoyl-L-tartaric acid; In methanol; for 0.5h; Purification / work up; Heating / reflux;

Reference yield:

: 2398-37-0
3-methoxyphenyl bromide

: 89920-95-6
N-benzyl-3(R)-(3-methoxyphenyl)piperidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium / iodine / diethyl ether / 1 h

1.2: 1 h / 20 - 30 °C

2.1: trifluoroacetic acid / Heating / reflux

3.1: hydrogen / palladium on activated charcoal / ethanol / 1.75 h / 2250.23 Torr

4.1: O,O'-dibenzoyl-L-tartaric acid / methanol / 0.5 h / Heating / reflux

With hydrogen; magnesium; O,O'-dibenzoyl-L-tartaric acid; trifluoroacetic acid; palladium on activated charcoal; iodine; In methanol; diethyl ether; ethanol;

Reference yield:

: 87996-59-6
1-benzyl-3-(3-methoxy-phenyl)-piperidin-3-ol

: 89920-95-6
N-benzyl-3(R)-(3-methoxyphenyl)piperidine

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / Heating / reflux

2: hydrogen / palladium on activated charcoal / ethanol / 1.75 h / 2250.23 Torr

3: O,O'-dibenzoyl-L-tartaric acid / methanol / 0.5 h / Heating / reflux

With hydrogen; O,O'-dibenzoyl-L-tartaric acid; trifluoroacetic acid; palladium on activated charcoal; In methanol; ethanol;