Benzenepentadecanoic acid, b-methyl-4-(1-piperidinylazo)-

Base Information

Chemical Name:Benzenepentadecanoic acid, b-methyl-4-(1-piperidinylazo)-
CAS No.:90046-97-2
Molecular Formula:C27H45N3O2
Molecular Weight:443.673
Hs Code.:

Synonyms:

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Chemical Property of Benzenepentadecanoic acid, b-methyl-4-(1-piperidinylazo)-

Chemical Property:

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Technology Process of Benzenepentadecanoic acid, b-methyl-4-(1-piperidinylazo)-

There total 10 articles about Benzenepentadecanoic acid, b-methyl-4-(1-piperidinylazo)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 90046-96-1
1-<4-(13(R,S)-Methyl-14-carbomethoxytetradecyl)-phenyl>-3,3-(1,5-pentanediyl)triazene

: 90046-97-2
1-<4-(13(R,S)-Methyl-14-carboxytetradecyl)-phenyl>-3,3-(1,5-pentanediyl)triazene

Guidance literature:: With sodium hydroxide; In ethanol; for 1h; Heating;
DOI:10.1021/jo00187a005

Reference yield:

: 4166-53-4
3-methylglutaric anhydride

: 90046-97-2
1-<4-(13(R,S)-Methyl-14-carboxytetradecyl)-phenyl>-3,3-(1,5-pentanediyl)triazene

Guidance literature:: Multi-step reaction with 10 steps

1: 90 h / 100 °C

2: SOCl₂ / 14 h / Ambient temperature

3: 83 percent / SnCl₄ / CH₂Cl₂ / 1.)0 deg C, 2.)R_.T_., 16 h

4: 90 percent / 85percent hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / Heating

5: 67 percent / Raney nickel, 10percent Na₂CO₃ / ethanol / 16 h / Heating

6: 96 percent / diethyl ether / 12 h / 0 °C

7: 1.)thallium(III) trifluoroacetate, trifluoracetic acid, 2.)isomayl nitrite, 12N HCl, AcOH / 1.)r.t., 48 h, 2.)CH₂Cl₂, red lights, 10 min.

8: 90 percent / NaBH₄ / Palladium on charcoal / methanol / 0.5 h / Ambient temperature

9: 1.)0.5N HCl, sodium nitrite / 1.)0-5 deg C, 5 min., 2.)H₂O, 0-5 deg C, 20 min.

10: 53 percent / 1N NaOH / ethanol / 1 h / Heating

With hydrogenchloride; potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; tin(IV) chloride; nickel; sodium carbonate; hydrazine hydrate; acetic acid; trifluoroacetic acid; sodium nitrite; isopentyl nitrite; thallium(III) trifluoroacetate; palladium on activated charcoal; In methanol; diethyl ether; ethanol; dichloromethane; diethylene glycol;
DOI:10.1021/jo00187a005

Reference yield:

: 27151-65-1
3-methyl-1,5-pentanedioic acid monomethyl ester

: 90046-97-2
1-<4-(13(R,S)-Methyl-14-carboxytetradecyl)-phenyl>-3,3-(1,5-pentanediyl)triazene

Guidance literature:: Multi-step reaction with 9 steps

1: SOCl₂ / 14 h / Ambient temperature

2: 83 percent / SnCl₄ / CH₂Cl₂ / 1.)0 deg C, 2.)R_.T_., 16 h

3: 90 percent / 85percent hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / Heating

4: 67 percent / Raney nickel, 10percent Na₂CO₃ / ethanol / 16 h / Heating

5: 96 percent / diethyl ether / 12 h / 0 °C

6: 1.)thallium(III) trifluoroacetate, trifluoracetic acid, 2.)isomayl nitrite, 12N HCl, AcOH / 1.)r.t., 48 h, 2.)CH₂Cl₂, red lights, 10 min.

7: 90 percent / NaBH₄ / Palladium on charcoal / methanol / 0.5 h / Ambient temperature

8: 1.)0.5N HCl, sodium nitrite / 1.)0-5 deg C, 5 min., 2.)H₂O, 0-5 deg C, 20 min.

9: 53 percent / 1N NaOH / ethanol / 1 h / Heating

With hydrogenchloride; potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; tin(IV) chloride; nickel; sodium carbonate; hydrazine hydrate; acetic acid; trifluoroacetic acid; sodium nitrite; isopentyl nitrite; thallium(III) trifluoroacetate; palladium on activated charcoal; In methanol; diethyl ether; ethanol; dichloromethane; diethylene glycol;
DOI:10.1021/jo00187a005