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6-Heptynoic acid, 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-, methyl ester, (S)-

Base Information Edit
  • Chemical Name:6-Heptynoic acid, 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-, methyl ester, (S)-
  • CAS No.:90108-29-5
  • Molecular Formula:C24H30O3Si
  • Molecular Weight:394.586
  • Hs Code.:
  • Mol file:90108-29-5.mol
6-Heptynoic acid, 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-, methyl ester,
(S)-

Synonyms:

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Chemical Property of 6-Heptynoic acid, 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-, methyl ester, (S)- Edit
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Technology Process of 6-Heptynoic acid, 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-, methyl ester, (S)-

There total 8 articles about 6-Heptynoic acid, 5-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-, methyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: 78 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1.5 h
2: 74 percent / imidazole / dimethylformamide / 48 h / Ambient temperature
With 1H-imidazole; tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(96)00316-X
Guidance literature:
Multi-step reaction with 4 steps
1: 60 percent / AlCl3 / CH2Cl2 / 0 °C
2: 85 percent / (-)-9-pinanyl-BBN / tetrahydrofuran / 25 °C
3: 80 percent / KF.2H2O / dimethylformamide
4: 96 percent / imidazole / dimethylformamide
With 1H-imidazole; potassium fluoride; aluminium trichloride; (-)-9-pinanyl-BBN; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00324a024
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