Phosphine sulfide, tris(2-methylphenyl)-

Base Information

• Chemical Name: Phosphine sulfide, tris(2-methylphenyl)-
• CAS No.: 6163-61-7
• Molecular Formula: C21H23PS
• Molecular Weight: 338.4461
• DSSTox Substance ID: DTXSID60210643
• Nikkaji Number: J465.634B
• Wikidata: Q83085405

Synonyms:Phosphine sulfide, tris(2-methylphenyl)-;Tris(2-methylphenyl)phosphine sulfide;6163-61-7;tri-o-tolyl phosphine sulfide;SCHEMBL7891692;DTXSID60210643

Chemical Property of Phosphine sulfide, tris(2-methylphenyl)-

Chemical Property:

• Boiling Point: 412.4°Cat760mmHg
• Flash Point: 214.6°C
• Density: g/cm³
• XLogP3: 6.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 336.11015884
• Heavy Atom Count: 23
• Complexity: 370

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=CC=C1P(=S)(C2=CC=CC=C2C)C3=CC=CC=C3C

Technology Process of Phosphine sulfide, tris(2-methylphenyl)-

There total 1 articles about Phosphine sulfide, tris(2-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tris-(o-tolyl)phosphine (6163-58-2) → tri(o-tolyl)phosphine sulphide (6163-61-7)

Guidance literature:

With sodium polisulfide; In methanol; acetone; for 0.0333333h; Ambient temperature;

DOI:10.1080/00397919208019299

Reference yield:

Cd(2+)*2SbF6(1-)=Cd(SbF6)2 + tri(o-tolyl)phosphine sulphide (6163-61-7) + tris(2-methylphenyl)phosphine selenide (32461-51-1) → Cd(SeP(C6H4CH3)3)2(SP(C6H4CH3)3)(2+) (75503-50-3)

Guidance literature:

In dichloromethane; the solvent removed by evapn. under N2, drying in vac.;

Reference yield:

Cd(2+)*2SbF6(1-)=Cd(SbF6)2 + tri(o-tolyl)phosphine sulphide (6163-61-7) + tris(2-methylphenyl)phosphine selenide (32461-51-1) → Cd(SeP(C6H4CH3)3)(SP(C6H4CH3)3)2(2+) (75503-49-0)

Guidance literature:

In dichloromethane; the solvent removed by evapn. under N2, drying in vac.;

upstream raw materials:

tris-(o-tolyl)phosphine

Downstream raw materials:

Cd(SeP(C₆H₄CH₃)3)2(SP(C₆H₄CH₃)3)⁽²⁺⁾

Cd(SeP(C₆H₄CH₃)3)(SP(C₆H₄CH₃)3)2⁽²⁺⁾

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