2-IMINO-3-METHYLCYCLOPENTANECARBONITRILE

Base Information

• Chemical Name: 2-IMINO-3-METHYLCYCLOPENTANECARBONITRILE
• CAS No.: 903631-60-7
• Molecular Formula: C₇H₁₀N₂
• Molecular Weight: 122.17
• Mol file: 903631-60-7.mol

Synonyms:2-IMINO-3-METHYLCYCLOPENTANECARBONITRILE;

Chemical Property of 2-IMINO-3-METHYLCYCLOPENTANECARBONITRILE

Chemical Property:

• PSA: 47.64000
• LogP: 1.67558

Purity/Quality:

2-IMINO-3-METHYLCYCLOPENTANECARBONITRILE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-IMINO-3-METHYLCYCLOPENTANECARBONITRILE

There total 2 articles about 2-IMINO-3-METHYLCYCLOPENTANECARBONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-adiponitrile (16525-39-6) → 2-imino-3-methylcyclopentanecarbonitrile (903631-60-7)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 5h; Heating;

DOI:10.1021/jf062845l

Reference yield:

hexanedinitrile (111-69-3) → 2-imino-3-methylcyclopentanecarbonitrile (903631-60-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 11.7 g / potassium tert-butoxide / tetrahydrofuran / 2.5 h / -10 - 20 °C

2: 3.2 g / NaH / tetrahydrofuran / 5 h / Heating

With potassium tert-butylate; sodium hydride; In tetrahydrofuran;

DOI:10.1021/jf062845l

upstream raw materials:

1-methyl-adiponitrile

hexanedinitrile