Benzenemethanamine, N-ethyl-4-(trifluoromethyl)-, hydrochloride

Base Information

• Chemical Name: Benzenemethanamine, N-ethyl-4-(trifluoromethyl)-, hydrochloride
• CAS No.: 90389-04-1
• Molecular Formula: C10H12F3N.ClH
• Molecular Weight: 239.668

Synonyms:

Chemical Property of Benzenemethanamine, N-ethyl-4-(trifluoromethyl)-, hydrochloride

Chemical Property:

• PSA: 12.03000
• LogP: 4.00780

Purity/Quality:

99% ^*data from raw suppliers

N-Ethyl-4-(trifluoromethyl)benzylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanamine, N-ethyl-4-(trifluoromethyl)-, hydrochloride

There total 2 articles about Benzenemethanamine, N-ethyl-4-(trifluoromethyl)-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-(4-(trifluoromethyl)benzyl)acetamide (637763-71-4) → Ethyl-(4-trifluoromethyl-benzyl)-amine; hydrochloride (90389-04-1)

Guidance literature:

N-(4-(trifluoromethyl)benzyl)acetamide; With phenylsilane-d3; C₃₆H₄₈F₆N₆NiO₅S₂; In toluene; at 110 ℃; for 24h; Inert atmosphere; Schlenk technique;

With hydrogenchloride; In diethyl ether;

DOI:10.1039/d1cc03537a

Reference yield:

p-Trifluoromethylbenzylamine (3300-51-4) → Ethyl-(4-trifluoromethyl-benzyl)-amine; hydrochloride (90389-04-1)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 20 °C

2: C₃₆H₄₈F₆N₆NiO₅S₂; phenylsilane-d3 / toluene / 24 h / 110 °C / Inert atmosphere; Schlenk technique

With phenylsilane-d3; C₃₆H₄₈F₆N₆NiO₅S₂; triethylamine; In dichloromethane; toluene;

DOI:10.1039/d1cc03537a

upstream raw materials:

p-Trifluoromethylbenzylamine

N-(4-(trifluoromethyl)benzyl)acetamide

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