Benzamide, 3,5-dibromo-N-(2,4-difluorophenyl)-2-methoxy-

Base Information

Chemical Name:Benzamide, 3,5-dibromo-N-(2,4-difluorophenyl)-2-methoxy-
CAS No.:90426-11-2
Molecular Formula:C14H9Br2F2NO2
Molecular Weight:421.036
Hs Code.:
DSSTox Substance ID:DTXSID70392101
Wikidata:Q82190044

Synonyms:90426-11-2;Benzamide, 3,5-dibromo-N-(2,4-difluorophenyl)-2-methoxy-;DTXSID70392101;AKOS003984481

Suppliers and Price of Benzamide, 3,5-dibromo-N-(2,4-difluorophenyl)-2-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Benzamide, 3,5-dibromo-N-(2,4-difluorophenyl)-2-methoxy-

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:420.89476
Heavy Atom Count:21
Complexity:375

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1Br)Br)C(=O)NC2=C(C=C(C=C2)F)F

Technology Process of Benzamide, 3,5-dibromo-N-(2,4-difluorophenyl)-2-methoxy-

There total 3 articles about Benzamide, 3,5-dibromo-N-(2,4-difluorophenyl)-2-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 79402-07-6
3,5-Dibromo-N-(2,4-difluoro-phenyl)-2-hydroxy-benzamide

: 77-78-1
dimethyl sulfate

: 90426-11-2
3,5-Dibromo-N-(2,4-difluoro-phenyl)-2-methoxy-benzamide

Guidance literature:: With sodium hydroxide; In diethylene glycol dimethyl ether; at 90 ℃; for 2h;
DOI:10.1248/cpb.32.305

Reference yield:

: 3147-55-5
3,5-dibromosalicylic acid

: 90426-11-2
3,5-Dibromo-N-(2,4-difluoro-phenyl)-2-methoxy-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / PCl₃ / xylene / 4 h / 140 °C

2: 59 percent / 2 N NaOH / bis-(2-methoxy-ethyl) ether / 2 h / 90 °C

With sodium hydroxide; phosphorus trichloride; In diethylene glycol dimethyl ether; xylene;
DOI:10.1248/cpb.32.305

Reference yield:

: 367-25-9,76563-56-9
2,4-difluorophenylamine

: 90426-11-2
3,5-Dibromo-N-(2,4-difluoro-phenyl)-2-methoxy-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / PCl₃ / xylene / 4 h / 140 °C

2: 59 percent / 2 N NaOH / bis-(2-methoxy-ethyl) ether / 2 h / 90 °C

With sodium hydroxide; phosphorus trichloride; In diethylene glycol dimethyl ether; xylene;
DOI:10.1248/cpb.32.305