3-Methoxyphenylglyoxal

Base Information

Chemical Name:3-Methoxyphenylglyoxal
CAS No.:32025-65-3
Molecular Formula:C9H8O3
Molecular Weight:164.161
Hs Code.:2914509090
DSSTox Substance ID:DTXSID70185853
Nikkaji Number:J3.144.483G
Wikidata:Q83056991
Mol file:32025-65-3.mol

Synonyms:3-methoxyphenylglyoxal;meta-methoxyphenylglyoxal

Suppliers and Price of 3-Methoxyphenylglyoxal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(3-Methoxyphenyl)glyoxal
100mg
$ 60.00

Crysdot
2-(3-Methoxyphenyl)-2-oxoacetaldehyde 95+%
25g
$ 357.00

American Custom Chemicals Corporation
3-METHOXYPHENYLGLYOXAL HYDRATE 95.00%
1G
$ 632.94

Alfa Aesar
3-Methoxyphenylglyoxal hydrate, 97%, dry wt. basis
5g
$ 198.00

Alfa Aesar
3-Methoxyphenylglyoxal hydrate, 97%, dry wt. basis
1g
$ 53.10

Absolute Chiral
3-Methoxyphenylglyoxalhydrate 95%
500 mg
$ 38.00

Total 12 raw suppliers

Chemical Property of 3-Methoxyphenylglyoxal

Chemical Property:

Vapor Pressure:0.00981mmHg at 25°C
Melting Point:99-100°C
Refractive Index:1.518
Boiling Point:264.3 °C at 760 mmHg
Flash Point:113.5 °C
PSA：52.60000
Density:1.153 g/cm³
LogP:1.01250
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:164.047344113
Heavy Atom Count:12
Complexity:177

Purity/Quality:

99% ^*data from raw suppliers

(3-Methoxyphenyl)glyoxal ^*data from reagent suppliers

Safty Information:

Pictogram(s): R36/37/38:Irritating to eyes, respiratory system and skin.;
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1)C(=O)C=O

Technology Process of 3-Methoxyphenylglyoxal

There total 4 articles about 3-Methoxyphenylglyoxal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 5000-65-7
2-bromo-3'-methoxyacetophenone

: 32025-65-3
3-methoxyphenylglyoxal

Guidance literature:: In water; dimethyl sulfoxide; at 20 ℃;
DOI:10.1016/j.bmcl.2017.06.078

Reference yield:

: 32025-65-3
3-methoxyphenylglyoxal

Guidance literature:: DOI:10.1021/jo00424a040

Reference yield:

: 87428-52-2
2-hydroxy-3'-methoxyacetophenone

: 32025-65-3
3-methoxyphenylglyoxal

Guidance literature:: 2-hydroxy-1-(3-methoxyphenyl)ethan-1-one; With copper(I) tetrakis(acetonitrile) hexafluorophosphate; for 0.5h; Molecular sieve; Schlenk technique;

With pyridine; oxygen; In methanol; at 20 ℃; for 0.5h; under 760.051 Torr; Schlenk technique; Molecular sieve;
DOI:10.1039/d2cc00773h