Technology Process of 1(3H)-Isobenzofuranone, 3-(3-methylphenyl)-
There total 14 articles about 1(3H)-Isobenzofuranone, 3-(3-methylphenyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chloro(1,5-cyclooctadiene)rhodium(I) dimer; Li2CO3; 1,2-bis-(diphenylphosphino)ethane;
In
water; 1,2-dichloro-ethane;
at 85 ℃;
for 12h;
DOI:10.1002/adsc.201000741
- Guidance literature:
-
With
chloro(1,5-cyclooctadiene)rhodium(I) dimer; oxygen; potassium carbonate; 1,4-di(diphenylphosphino)-butane;
In
1,2-dichloro-ethane;
at 65 ℃;
for 12h;
DOI:10.1002/anie.201000302
- Guidance literature:
-
N-methylbenzamide; m-tolyl aldehyde;
With
rhenium(I) pentacarbonyl bromide; dimethyl zinc(II); zinc dibromide;
In
1,2-dimethoxyethane; toluene;
at 130 ℃;
for 24h;
Inert atmosphere;
Schlenk technique;
With
hydrogenchloride;
In
1,2-dimethoxyethane; water; toluene;
at 80 ℃;
for 3h;
chemoselective reaction;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/acs.orglett.9b02142
