Technology Process of 12-Methoxy-1,4,12-trioxododecan-2-yl benzoate
There total 5 articles about 12-Methoxy-1,4,12-trioxododecan-2-yl benzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 70 percent / hydroxylamine hydrochloride, sodium bicarbonate / H2O / 24 h
2: 46 percent
3: H2 / Ra-Ni / aq. ethanol / 4 h / Ambient temperature
4: 80 percent / pyridine / 50 h / 25 °C
5: 80 percent / CCl4; formic acid / 0.58 h / 25 °C
With
hydroxylamine hydrochloride; hydrogen; sodium hydrogencarbonate;
Ra-Ni;
In
pyridine; tetrachloromethane; formic acid; ethanol; water;
DOI:10.1016/S0040-4020(01)91249-9
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 46 percent
2: H2 / Ra-Ni / aq. ethanol / 4 h / Ambient temperature
3: 80 percent / pyridine / 50 h / 25 °C
4: 80 percent / CCl4; formic acid / 0.58 h / 25 °C
With
hydrogen;
Ra-Ni;
In
pyridine; tetrachloromethane; formic acid; ethanol;
DOI:10.1016/S0040-4020(01)91249-9
