Technology Process of Pyrrolidine,
1-[(hexahydro-1,3-dioxo-2-phenyl-1H-pyrrolo[1,2-c]imidazol-5-yl)carbon
yl]-
There total 8 articles about Pyrrolidine,
1-[(hexahydro-1,3-dioxo-2-phenyl-1H-pyrrolo[1,2-c]imidazol-5-yl)carbon
yl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 94 percent / diethyl ether / 1 h / Heating; 1.) room temp., 15 min
2: 18percent HCl / H2O / 90 h / Heating
4: 1.) ethyl chloroformate, triethylamine / 1.) benzene, ether, 0 deg C, 15 min; 2.) benzene, ether, room temp. 20 min
With
hydrogenchloride; chloroformic acid ethyl ester; triethylamine;
In
diethyl ether; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 94 percent / diethyl ether / 1 h / Heating; 1.) room temp., 15 min
2: 18percent HCl / H2O / 90 h / Heating
4: 1.) ethyl chloroformate, triethylamine / 1.) benzene, ether, 0 deg C, 15 min; 2.) benzene, ether, room temp. 20 min
With
hydrogenchloride; chloroformic acid ethyl ester; triethylamine;
In
diethyl ether; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 18percent HCl / H2O / 90 h / Heating
3: 1.) ethyl chloroformate, triethylamine / 1.) benzene, ether, 0 deg C, 15 min; 2.) benzene, ether, room temp. 20 min
With
hydrogenchloride; chloroformic acid ethyl ester; triethylamine;
In
water;
