Borane, (2,4,6-trimethylphenyl)bis(triphenylsilyl)-

Base Information

Chemical Name:Borane, (2,4,6-trimethylphenyl)bis(triphenylsilyl)-
CAS No.:90670-76-1
Molecular Formula:C₄₅H₄₁BSi₂
Molecular Weight:648.803
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Borane, (2,4,6-trimethylphenyl)bis(triphenylsilyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Borane, (2,4,6-trimethylphenyl)bis(triphenylsilyl)-

There total 1 articles about Borane, (2,4,6-trimethylphenyl)bis(triphenylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: triphenylsilyl lithium

: mesityl boron dibromide

: 90670-76-1
mesityl-bis(triphenylsilyl)borane

Guidance literature:: In tetrahydrofuran; n-heptane; byproducts: LiBr; adding Ph3SiLi in THF to a soln. of (C6H2(CH3)3)BBr2 in heptane (-10°C), stirring (24 h, room temp.); evapg., dissolving (hot heptane), filtering, cooling to -15°C, pptn., recrystn. (several times, heptane); elem. anal.;

Reference yield:

: 90670-76-1
mesityl-bis(triphenylsilyl)borane

: 5980-97-2
mesitylboronic acid

Guidance literature:: With water; In not given;

Reference yield:

: 90670-76-1
mesityl-bis(triphenylsilyl)borane

: 96-14-0
3-methylpentane

: 90670-78-3
3-methylpentyl(triphenylsilyl)borane

Guidance literature:: In solid matrix; byproducts: (mesityl)SiPh3; Irradiation (UV/VIS); irradiating in a 3-methylpentane matrix (-196°C, 254 nm), thawing;