Cyclopropanecarboxaldehyde, 3-(4-methoxyphenyl)-2,2-bis(phenylthio)-, trans-

Base Information

Chemical Name:Cyclopropanecarboxaldehyde, 3-(4-methoxyphenyl)-2,2-bis(phenylthio)-, trans-
CAS No.:90714-17-3
Molecular Formula:C23H20O2S2
Molecular Weight:392.543
Hs Code.:

Synonyms:

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Chemical Property of Cyclopropanecarboxaldehyde, 3-(4-methoxyphenyl)-2,2-bis(phenylthio)-, trans-

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Technology Process of Cyclopropanecarboxaldehyde, 3-(4-methoxyphenyl)-2,2-bis(phenylthio)-, trans-

There total 3 articles about Cyclopropanecarboxaldehyde, 3-(4-methoxyphenyl)-2,2-bis(phenylthio)-, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 90714-14-0
3-(p-anisyl)-1-formyl-2,2-dichlorocyclopropane

: 108-98-5
thiophenol

: 90714-17-3
3-(p-anisyl)-2,2-diphenylthio-1-formylcyclopropane

Guidance literature:: With sodium methylate; In methanol; at 20 - 25 ℃; for 0.25h;

Reference yield:

: 71277-02-6,72233-10-4,24056-43-7
3,3-Diethoxy-1-(4-methoxyphenyl)-1-propen

: 90714-17-3
3-(p-anisyl)-2,2-diphenylthio-1-formylcyclopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / 50percent aq. NaOH, TEBA / CHCl₃

2: 71 percent / oxalic acid / H₂O; dioxane / 0.5 h / Heating

3: 60 percent / sodium methoxide / methanol / 0.25 h / 20 - 25 °C

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; sodium methylate; oxalic acid; In 1,4-dioxane; methanol; chloroform; water;

Reference yield:

: 60682-78-2,90714-10-6
3-(p-anisyl)-2,2-dichloro-1-diethoxymethylcyclopropane

: 90714-17-3
3-(p-anisyl)-2,2-diphenylthio-1-formylcyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / oxalic acid / H₂O; dioxane / 0.5 h / Heating

2: 60 percent / sodium methoxide / methanol / 0.25 h / 20 - 25 °C

With sodium methylate; oxalic acid; In 1,4-dioxane; methanol; water;